2,6-二甲基-1,2,3,4,4a,5,6,7,8,8a-十氢萘合成路线 (共 2 条)
→
1618-22-02,6-二甲基-1,2,3,4,4a,5,6,7,8,8a-十氢萘
反应条件
ammonia; sulfur; molybdenum(VI) oxide T=390 - 400°C; P=73550.8 Torr; Hydrogenation.Reagens 4: Aktivkohle;
参考文献
Coulson
Journal of the Chemical Society, 1935 , p. 77,81
→
1618-22-02,6-二甲基-1,2,3,4,4a,5,6,7,8,8a-十氢萘+
反应条件
aluminum tri-bromide in neat (no solvent) T=20°C; 1 h; other solvent and temperature; Product distribution;
参考文献
Akhrem, I.S.; Orlinkov, A.V.; Mysov, E.I.; Vol'pin, M.E.
Tetrahedron Letters, 1981 , vol. 22, # 39 p. 3891 - 3894