反应条件
1: 2-chloro-6-methyl-pyridine With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran T=-78°C; Inert atmosphere; 2: carbonic acid dimethyl ester in tetrahydrofuran T=-78 - 20°C; Inert atmosphere;
参考文献
INCEPTION 2, INC.; STOCK, Nicholas, Simon; CHEN, Austin, Chih-Yu; BRAVO, Yalda, Mostofi; JACINTHO, Jason, Duarte; SCOTT, Jill, Melissa; STEARNS, Brian, Andrew; CLARK, Ryan, Christopher; TRUONG, Yen, Pham
Patent: WO2013/134562 A1, 2013 ;
Location in patent: Paragraph 00202 ;
