N-(4-甲基苄基)-1-丁胺合成路线 （共 5 条）
反应条件
sodium tetrahydroborate; 2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride 1.) cyclohexane, 2 h, reflux; 2.) DMF/cyclohexane, r.t.; Yield given. Multistep reaction;
参考文献
Bowman, W.Russell; Clark, David N.; Marmon, Robert J.
Tetrahedron Letters, 1991 , vol. 32, # 44 p. 6441 - 6444
反应条件
1: p-TsOH / toluene / 2 h / Heating 2: NaBH4 / methanol / 2 h / Heating 3: 44 percent / toluene / 1 h / Heating 4: 1.) Bu3SnH, AIBN; 2.) NaBH4 / 1.) cyclohexane, 2 h, reflux; 2.) DMF/cyclohexane, r.t. View Scheme
参考文献
Bowman, W. Russell; Clark, David N.; Marmon, Robert J.
Tetrahedron, 1994 , vol. 50, # 4 p. 1275 - 1294
反应条件
1: NaBH4 / methanol / 2 h / Heating 2: 44 percent / toluene / 1 h / Heating 3: 1.) Bu3SnH, AIBN; 2.) NaBH4 / 1.) cyclohexane, 2 h, reflux; 2.) DMF/cyclohexane, r.t. View Scheme
参考文献
Bowman, W. Russell; Clark, David N.; Marmon, Robert J.
Tetrahedron, 1994 , vol. 50, # 4 p. 1275 - 1294
反应条件
sodium tetrahydroborate; tin(IV) chloride 1.) CH2Cl2, 2.) MeOH; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Pearson, William H.; Fang, Wen-kui
Journal of Organic Chemistry, 1995 , vol. 60, # 16 p. 4960 - 4961
反应条件
in nitrobenzene T=40°C; Rate constantMechanism;
参考文献
Bowman, W. Russell; Clark, David N.; Marmon, Robert J.
Tetrahedron, 1994 , vol. 50, # 4 p. 1275 - 1294
