2,2-二氟苯并[d][1,3]二氧代-4-甲腈合成路线 （共 7 条）
反应条件
pyridine; 2,4,6-trichloro-1,3,5-triazine in dichloromethane T=25°C; 2 h;
参考文献
Schlosser, Manfred; Gorecka, Joanna; Castagnetti, Eva
European Journal of Organic Chemistry, 2003 , # 3 p. 452 - 462
反应条件
ammonia; iodine in tetrahydrofuran; water T=25°C; 2 h;
参考文献
Schlosser, Manfred; Gorecka, Joanna; Castagnetti, Eva
European Journal of Organic Chemistry, 2003 , # 3 p. 452 - 462
反应条件
thionyl chloride 6 h; Heating;
参考文献
Schlosser, Manfred; Gorecka, Joanna; Castagnetti, Eva
European Journal of Organic Chemistry, 2003 , # 3 p. 452 - 462
反应条件
1: 88 percent / sec-butyllithium / tetrahydrofuran; cyclohexane / -75 °C 2: 68 percent / iodine; ammonia / tetrahydrofuran; H2O / 2 h / 25 °C View Scheme
参考文献
Schlosser, Manfred; Gorecka, Joanna; Castagnetti, Eva
European Journal of Organic Chemistry, 2003 , # 3 p. 452 - 462
反应条件
1: 90 percent / boron trifluoride-diethyl etherate / 48 h / 25 °C 2: 56 percent / formamide; sodium methoxide / dimethylformamide / 6 h / 100 °C 3: 91 percent / thionyl chloride / 6 h / Heating View Scheme
参考文献
Schlosser, Manfred; Gorecka, Joanna; Castagnetti, Eva
European Journal of Organic Chemistry, 2003 , # 3 p. 452 - 462
反应条件
1: 92 percent / ammonia / H2O 2: 91 percent / thionyl chloride / 6 h / Heating View Scheme
参考文献
Schlosser, Manfred; Gorecka, Joanna; Castagnetti, Eva
European Journal of Organic Chemistry, 2003 , # 3 p. 452 - 462
反应条件
1: 56 percent / formamide; sodium methoxide / dimethylformamide / 6 h / 100 °C 2: 91 percent / thionyl chloride / 6 h / Heating View Scheme
参考文献
Schlosser, Manfred; Gorecka, Joanna; Castagnetti, Eva
European Journal of Organic Chemistry, 2003 , # 3 p. 452 - 462
