2,2-二乙基乙酰乙酸乙酯合成路线 (共 36 条)
反应条件
P(MeNCH2CH2)3N in hexane; acetonitrile T=0°C; 0.5 h;
参考文献
Arumugam, Subramaniam; McLeod, Dale; Verkade, John G.
Journal of Organic Chemistry, 1998 , vol. 63, # 11 p. 3677 - 3679
反应条件
tetra-(n-butyl)ammonium iodide; potassium carbonate in N,N-dimethyl-formamide T=20°C; Inert atmosphere;
参考文献
Viera, Ignacio; Manta, Eduardo; Gonzalez, Lucia; Mahler, Graciela
Tetrahedron Asymmetry, 2010 , vol. 21, # 5 p. 631 - 635
反应条件
1: potassium tert-pentylate 2: potassium tert-pentylate View Scheme
参考文献
Journal of the American Chemical Society, , vol. 66, p. 145
反应条件
potassium 2-methyl-2-butoxide
参考文献
Journal of the American Chemical Society, , vol. 66, p. 145
参考文献
Journal of the American Chemical Society, , vol. 60, p. 131
反应条件
sodium hydride; N,N-dimethyl-formamide; benzene anschliessend mit Aethyljodid;
参考文献
Journal of Organic Chemistry, , vol. 21, p. 245
反应条件
aluminum oxide; sodium ethanolate 2.) room temperature, 5 d; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bram, G.; Fillebeen-Khan, T.; Geraghty, N.
Synthetic Communications, 1980 , vol. 10, # 4 p. 279 - 290
参考文献
Tetrahedron, , vol. 27, p. 4777 - 4785
反应条件
sodium methylate in dichloromethane T=20°C; 0.15 h;
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 11-12 p. 431 - 434
反应条件
1: benzene 2: benzene; sodium View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 186, p. 201,208