4-甲基-联苯-2-甲醛合成路线 （共 29 条）
反应条件
potassium hydroxide; C13H16NO4S(1-)*Na(1+); palladium dichloride in water T=100°C; Suzuki coupling; 2 h;
参考文献
Guo, Xuming; Zhou, Jin; Li, Xiaoyan; Sun, Hongjian
Journal of Organometallic Chemistry, 2008 , vol. 693, # 25 p. 3692 - 3696
反应条件
1,1,3,3-tetramethyldisiloxane; vanadium triisopropoxide oxide in toluene T=60°C; 20 h;
参考文献
Laval, Stephane; Dayoub, Wissam; Pehlivan, Leyla; Metay, Estelle; Delbrayelle, Dominique; Mignani, Gerard; Lemaire, Marc
Tetrahedron Letters, 2014 , vol. 55, # 1 p. 23 - 26
反应条件
sodium hydroxide; PEG encapsulated palladium nanoparticle in water T=90°C; Hiyama cross-coupling reaction; 3.5 h;
参考文献
Srimani, Dipankar; Sawoo, Sudeshna; Sarkar, Amitabha
Organic Letters, 2007 , vol. 9, # 18 p. 3639 - 3642
反应条件
quinoline; copper(I) bromide; palladium (II) bromide; biphenyl-2-yl-di-tert-butyl-phosphane in 1-methyl-pyrrolidin-2-one T=170°C; 24 h;
参考文献
Goossen, Lukas J.; Zimmermann, Bettina; Knauber, Thomas
Angewandte Chemie - International Edition, 2008 , vol. 47, # 37 p. 7103 - 7106
反应条件
caesium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether Suzuki-Miyaura coupling; 20 h; Heating;
参考文献
Li, Guijie; Wang, Erjuan; Chen, Haoyi; Li, Hongfeng; Liu, Yuanhong; Wang, Peng George
Tetrahedron, 2008 , vol. 64, # 38 p. 9033 - 9043
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; potassium fluoride; C58H47P in tetrahydrofuran Suzuki-Miyaura coupling; 14 h; Inert atmosphereReflux;
参考文献
Iwasawa, Tetsuo; Kamei, Toshinori; Watanabe, Satoshi; Nishiuchi, Masaki; Kawamura, Yasuhiko
Tetrahedron Letters, 2008 , vol. 49, # 52 p. 7430 - 7433
反应条件
1: 2-Carboxybenzaldehyde With potassium carbonate in various solvent(s) T=120°C; 0.5 h; 2: para-bromotoluene With 1,10-phenanthroline; copper(I) bromide in various solvent(s) T=170°C; 24 h; Further stages.;
参考文献
Goossen, Lukas J.; Rodriguez, Nuria; Melzer, Bettina; Linder, Christophe; Deng, Guojun; Levy, Laura M.
Journal of the American Chemical Society, 2007 , vol. 129, # 15 p. 4824 - 4833
反应条件
1: 42.55 g / diisobutylaluminum hydride / toluene / 0.25 h / -78 - -70 °C 2: pyridinium chlorochromate / CH2Cl2 / 0.5 h / 25 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 8 p. 2525 - 2547
反应条件
2,2'-bis(di-p-tolyl-phosphino)-1,1'-binaphthyl; copper(I) oxide; 1,10-phenanthroline; palladium (II) 2,4-pentanedionate in 1-methyl-pyrrolidin-2-one T=50 - 190°C; P=3375.34 Torr; Inert atmosphereMicrowave irradiation;
参考文献
Goossen, Lukas J.; Linder, Christophe; Rodriguez, Nuria; Lange, Paul P.
Chemistry - A European Journal, 2009 , vol. 15, # 37 p. 9336 - 9349
反应条件
copper(I) oxide; bis(acetylacetonato) palladium; copper(l) iodide; 1,10-phenanthroline in 1-methyl-pyrrolidin-2-one; quinoline T=50 - 190°C; 0.25 h; Inert atmosphereMicrowave irradiation;
参考文献
Goossen, Lukas J.; Linder, Bettina Zimmermanns Christophe; Rodriguez, Nuria; Lange, Paul P.; Hartung, Jens
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 16 p. 2667 - 2674
