(2-氨基苄基)-氨基甲酸叔丁酯合成路线 （共 5 条）
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=20°C; 2 h; Inert atmosphere;
参考文献
Brady, Ryan M.; Khakham, Yelena; Lessene, Guillaume; Baell, Jonathan B.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 3 p. 656 - 658
反应条件
water; iron; ammonium chloride in ethanol 1 h; Heating / reflux;
参考文献
Nihon Nohyaku Co., Ltd.
Patent: JP2005/314407 A, 2005 ;
Location in patent: Page/Page column 57 ;
反应条件
1: triethylamine / dichloromethane / 3 h / 20 °C 2: palladium 10 on activated carbon; hydrogen / ethyl acetate / 1 h View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 19, # 5 p. 1623 - 1642
反应条件
1: triethylamine / dichloromethane / 3 h / 20 °C 2: palladium 10 on activated carbon; hydrogen / ethyl acetate / 1 h View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 19, # 5 p. 1623 - 1642
反应条件
1: N-ethyl-N,N-diisopropylamine / acetonitrile / 0.25 h / 0 - 20 °C
2: trifluoroacetic acid / dichloromethane
3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 60 °C
View Scheme
参考文献
Brady, Ryan M.; Khakham, Yelena; Lessene, Guillaume; Baell, Jonathan B.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 3 p. 656 - 658
