1,2-/1,4-二甲基金刚烷合成路线 (共 14 条)
反应条件
Y-zeolite(Na/H 0.4) in hexane T=300°C; 30 h; ConcentrationTime;
参考文献
Khusnutdinov; Kislitsina; Khazipova; Kutepov
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 9 p. 1273 - 1278
Zh. Org. Khim., 2013 , vol. 49, # 9 p. 1290 - 1295,6
反应条件
Y-zeolite(Na/H 0.97) in hexane T=320°C; 3 h;
参考文献
Khusnutdinov; Kislitsina; Khazipova; Kutepov
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 9 p. 1273 - 1278
Zh. Org. Khim., 2013 , vol. 49, # 9 p. 1290 - 1295,6
反应条件
hydrogen; sodium methylate; nickel in methanol
参考文献
Yurchenko,A.G. et al.
Journal of Organic Chemistry USSR (English Translation), 1972 , vol. 8, p. 2380 - 2385
Zhurnal Organicheskoi Khimii, 1972 , vol. 8, # 11 p. 2332 - 2338
反应条件
1: HBr / CCl4 2: H2, NaOMe / Raney-Ni / methanol View Scheme
参考文献
Yurchenko,A.G. et al.
Journal of Organic Chemistry USSR (English Translation), 1972 , vol. 8, p. 2380 - 2385
Zhurnal Organicheskoi Khimii, 1972 , vol. 8, # 11 p. 2332 - 2338
反应条件
lithium in hexane; tert-butyl alcohol
参考文献
Landa,S.; Hlavaty,J.
Collection of Czechoslovak Chemical Communications, 1971 , vol. 36, p. 3059 - 3065
反应条件
1: H2SO4 2: LiAlH4 / diethyl ether 3: SOBr2 / Heating 4: Li / hexane; 2-methyl-propan-2-ol View Scheme
参考文献
Landa,S.; Hlavaty,J.
Collection of Czechoslovak Chemical Communications, 1971 , vol. 36, p. 3059 - 3065
反应条件
1: LiAlH4 / diethyl ether 2: SOBr2 / Heating 3: Li / hexane; 2-methyl-propan-2-ol View Scheme
参考文献
Landa,S.; Hlavaty,J.
Collection of Czechoslovak Chemical Communications, 1971 , vol. 36, p. 3059 - 3065
反应条件
1: SOBr2 / Heating 2: Li / hexane; 2-methyl-propan-2-ol View Scheme
参考文献
Landa,S.; Hlavaty,J.
Collection of Czechoslovak Chemical Communications, 1971 , vol. 36, p. 3059 - 3065
反应条件
1: hydrogen / hexane / 3 h / 20 °C / 76005.1 Torr / |Autoclave 2: Y-zeolite(Na/H 0.4) / hexane / 10 h / 300 °C 3: Y-zeolite(Na/H 0.97) / hexane / 3 h / 320 °C View Scheme
参考文献
Khusnutdinov; Kislitsina; Khazipova; Kutepov
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 9 p. 1273 - 1278
Zh. Org. Khim., 2013 , vol. 49, # 9 p. 1290 - 1295,6
反应条件
1: hydrogen / hexane / 3 h / 20 °C / 76005.1 Torr / |Autoclave 2: Y-zeolite(Na/H 0.4) / hexane / 10 h / 300 °C View Scheme
参考文献
Khusnutdinov; Kislitsina; Khazipova; Kutepov
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 9 p. 1273 - 1278
Zh. Org. Khim., 2013 , vol. 49, # 9 p. 1290 - 1295,6