1: benzenesulphinic acid sodium salt With polystyrene-supported-SeCl in N,N-dimethyl-formamide T=20°C; 6 h; solid-phase reaction; 2: styrene With 2,2'-azo-bisisobutyronitrile in benzene 20 h; Heating; 3: With dihydrogen peroxide in tetrahydrofuran T=20°C; 2 h;
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium acetate in N,N-dimethyl-formamide T=135°C; Heck-type olefination; 12 h;
参考文献
Na, Youngim; Park, Soyoung; Han, Soo Bong; Han, Hoon; Ko, Sangwon; Chang, Sukbok
Journal of the American Chemical Society, 2004 , vol. 126, # 1 p. 250 - 258