1: With tris-(2-chloro-ethyl)-amine; triphenylphosphine; diethylazodicarboxylate in benzene T=23°C; azidation; 15 h; 2: With lithium aluminium tetrahydride in tetrahydrofuran T=0 - 23°C; Reduction; 1.5 h; Further stages.;
参考文献
Coffey, D. Scott; McDonald, Andrew I.; Overman, Larry E.; Rabinowitz, Michael H.; Renhowe, Paul A.
Journal of the American Chemical Society, 2000 , vol. 122, # 20 p. 4893 - 4903