1-(2-甲基苯基)-2-苯乙酮合成路线 （共 35 条）
反应条件
sulfur nitride in toluene 24 h; Heating;
参考文献
Mataka, Shuntaro; Hosoki, Akira; Takahashi, Kazufumi; Tashiro, Masashi
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 1681 - 1685
反应条件
dipyridinium dichromate in dichloromethane
参考文献
Wessig, Pablo; Glombitza, Clemens; Mueller, Gunnar; Teubner, Janek
Journal of Organic Chemistry, 2004 , vol. 69, # 22 p. 7582 - 7591
反应条件
1: With sodium hydrogencarbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide
T=150°C; Heck reaction; 20 h;
2: With hydrogenchloride in tetrahydrofuran
T=25°C; Further stages.;
参考文献
Battace, Ahmed; Feuerstein, Marie; Lemhadri, Mhamed; Zair, Touriya; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2007 , # 19 p. 3122 - 3132
反应条件
ammonium chloride; bipyridine-cyclopalladated ferrocenylimine complex in water
T=100°C; 24 h;
参考文献
Yu, Ajuan; Li, Jingya; Cui, Mengjun; Wu, Yangjie
Synlett, 2007 , # 19 p. 3063 - 3067
反应条件
[Pd(0)(iPr2PCB11H5Br6)2][Li(THF)4]2; sodium t-butanolate in tetrahydrofuran
T=80°C; 6 h;
参考文献
THE REGENTS OF THE UNIVERSITY OF CALIFORNIA; LAVALLO, Vincent
Patent: WO2014/71401 A1, 2014 ;
Location in patent: Paragraph 0164; 0165 ;
反应条件
palladium diacetate; 1,4-di(diphenylphosphino)-butane in tetrahydrofuran
T=90°C; P=1500.15 Torr; 1 h; Sealed tubeMicrowave irradiation; chemoselective reaction;
参考文献
Motwani, Hitesh V.; Larhed, Mats
European Journal of Organic Chemistry, 2013 , # 22 p. 4729 - 4733
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); 1,8-diazabicyclo[5.4.0]undec-7-ene; [(t-Bu)3PH]BF4 in tetrahydrofuran
T=120°C; P=2250.23 Torr; 0.5 h; Microwave irradiationSealed tube; chemoselective reaction;
参考文献
Motwani, Hitesh V.; Larhed, Mats
European Journal of Organic Chemistry, 2013 , # 22 p. 4729 - 4733
反应条件
lithium bromide in diethyl ether
T=0°C;
参考文献
Loeschorn, Carol A.; Nakajima, Masayuki; Anselme, Jean-Pierre
Bulletin des Societes Chimiques Belges, 1981 , vol. 90, # 9 p. 985 - 986
反应条件
Ni(PCy3)2Cl2; sodium t-butanolate in N,N-dimethyl-formamide; toluene
T=100°C; Suzuki-Miyaura coupling; 0.666667 h; Inert atmosphere;
参考文献
Huang, Kun; Li, Gang; Huang, Wei-Ping; Yu, Da-Gang; Shi, Zhang-Jie
Chemical Communications, 2011 , vol. 47, # 25 p. 7224 - 7226
反应条件
palladium diacetate; 1,4-di(diphenylphosphino)-butane; zinc in 1,4-dioxane
T=100°C; Negishi coupling reaction; P=7500.75 Torr; 16 h; Inert atmosphereAutoclave;
参考文献
Wu, Xiao-Feng; Schranck, Johannes; Neumann, Helfried; Beller, Matthias
Chemistry - An Asian Journal, 2012 , vol. 7, # 1 p. 40 - 44
