1-(2-甲基苯基)-2-苯乙酮合成路线 （共 35 条）
反应条件
NaX zeolite in pentane
2 h; Irradiation; Further byproducts given;
参考文献
Ramamurthy, V.; Corbin, D. R.; Turro, N. J.; Zhang, Z.; Garcia-Garibay, M. A.
Journal of Organic Chemistry, 1991 , vol. 56, # 1 p. 255 - 261
反应条件
1: NaHCO3; Tedicyp / [PdCl(C3H5)]2 / dimethylformamide / 20 h / 150 °C
2: 79 percent / HCl / tetrahydrofuran; H2O / 25 °C
View Scheme
参考文献
Battace, Ahmed; Zair, Touriya; Doucet, Henri; Santelli, Maurice
Tetrahedron Letters, 2006 , vol. 47, # 4 p. 459 - 462
反应条件
1: NaHCO3; Tedicyp / [PdCl(C3H5)]2 / dimethylformamide / 20 h / 150 °C
2: 79 percent / HCl / tetrahydrofuran; H2O / 25 °C
View Scheme
参考文献
Battace, Ahmed; Zair, Touriya; Doucet, Henri; Santelli, Maurice
Tetrahedron Letters, 2006 , vol. 47, # 4 p. 459 - 462
反应条件
1.1: Mg; iodine / diethyl ether
1.2: 95 percent / diethyl ether / 1 h
2.1: 89 percent / PDC / CH2Cl2
View Scheme
参考文献
Wessig, Pablo; Glombitza, Clemens; Mueller, Gunnar; Teubner, Janek
Journal of Organic Chemistry, 2004 , vol. 69, # 22 p. 7582 - 7591
反应条件
in tetrahydrofuran; water
T=50°C; 48 h;
参考文献
Aggarwal, Varinder K.; De Vicente, Javier; Pelotier, Beatrice; Holmes, Ian P.; Bonnert, Roger V.
Tetrahedron Letters, 2000 , vol. 41, # 52 p. 10327 - 10331
反应条件
1: 59 percent / diethyl ether / 3 h / 0 °C
2: 65 percent / pyridinium dichromate (PDC) / dimethylformamide / 3 h / 0 °C
View Scheme
参考文献
Anstead, Gregory M.; Peterson, Chad S.; Pinney, Kevin G.; Wilson, Scott R.; Katzenellenbogen, John A.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 10 p. 2726 - 2734
参考文献
Eastham; Raaen
Proceedings of the Chemical Society, London, 1958 , p. 149
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Raaen; Eastham
Journal of the American Chemical Society, 1960 , vol. 82, p. 1349,1351
反应条件
[rhenium(pentacarbonyl)(bromide)]
2 h; Heating;
参考文献
Kusama, Hiroyuki; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 8 p. 2379 - 2384
反应条件
1.1: Mg; iodine / diethyl ether
1.2: 95 percent / diethyl ether / 1 h
2.1: 89 percent / PDC / CH2Cl2
View Scheme
参考文献
Wessig, Pablo; Glombitza, Clemens; Mueller, Gunnar; Teubner, Janek
Journal of Organic Chemistry, 2004 , vol. 69, # 22 p. 7582 - 7591
反应条件
in diethyl ether
20 h;
参考文献
Brouw, P. M. op den; Laarhoven, W. H.
Recueil: Journal of the Royal Netherlands Chemical Society, 1982 , vol. 101, # 2 p. 58 - 67
