[(环己基氧基)甲基]苯合成路线 (共 80 条)
反应条件
tin(II) trifluoromethanesulfonate; dimethyl tert-butyl silane in acetonitrile
T=-20°C;
参考文献
Suzuki, Takeshi; Oriyama, Takeshi
Synthetic Communications, 1999 , vol. 29, # 8 p. 1263 - 1269
反应条件
triethylsilane; iron(III) chloride in nitromethane
T=0 - 20°C; 0.666667 h;
参考文献
Iwanami, Katsuyuki; Yano, Kentaro; Oriyama, Takeshi
Synthesis, 2005 , # 16 art. no. F05505SS, p. 2669 - 2672
反应条件
triethylsilane; iron(III) chloride in nitromethane
T=20°C; 1 h;
参考文献
Iwanami, Katsuyuki; Yano, Kentaro; Oriyama, Takeshi
Chemistry Letters, 2007 , vol. 36, # 1 p. 38 - 39
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=0°C; Inert atmosphere; regioselective reaction;
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
1: PhBF3(-)K(+) With boron trifluoride diethyl etherate in dichloromethane
T=0°C; 0.5 h; Inert atmosphere;
2: 2-(cyclohexyloxymethoxy)-N,N-dimethylacetamide in dichloromethane
T=23°C; Inert atmosphere; regioselective reaction;
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
1: PhBF3(-)K(+) With boron trifluoride diethyl etherate in dichloromethane
T=0°C; 0.5 h; Inert atmosphere;
2: 2-((cyclohexyloxymethoxy)methyl)pyridine in dichloromethane
T=23°C; Inert atmosphere; regioselective reaction;
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
1: PhBF3(-)K(+) With boron trifluoride diethyl etherate in dichloromethane
T=0°C; 0.5 h; Inert atmosphere;
2: ethyl 2-(cyclohexyloxymethoxy)acetate in dichloromethane
T=23°C; Inert atmosphere; regioselective reaction;
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
trimethylsilyl trifluoromethanesulfonate in chloroform
T=20°C; 4 h;
参考文献
Kobashi, Yohei; Minowa, Tomofumi; Mukaiyama, Teruaki
Chemistry Letters, 2004 , vol. 33, # 10 art. no. CL-040929, p. 1362 - 1363
反应条件
1: PhBF3(-)K(+) With boron trifluoride diethyl etherate in dichloromethane
T=0°C; 0.5 h; Inert atmosphere;
2: 1-(cyclohexyloxymethoxy)-2-methoxybenzene in dichloromethane
T=23°C; Inert atmosphere; regioselective reaction;
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
1: PhBF3(-)K(+) With boron trifluoride diethyl etherate in dichloromethane
T=0°C; 0.5 h; Inert atmosphere;
2: 2-(cyclohexyloxymethoxy)isoindoline-1,3-dione in dichloromethane
T=40°C; 1.5 h; Inert atmosphere; regioselective reaction;
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089