[(环己基氧基)甲基]苯合成路线 （共 80 条）
反应条件
potassium hydroxide; tetrafluoroboric acid; mercury(II) oxide in dichloromethane
1.) room temp., 1 h;
参考文献
Barluenga, Jose; Alonso-Cires, Luisa; Campos, Pedro J.; Asensio, Gregorio
Synthesis, 1983 , # 1 p. 53 - 55
反应条件
PPh3 gold(I) chloro complex; silver trifluoromethanesulfonate in chlorobenzene
T=20°C; 3 h; Inert atmosphere;
参考文献
Aikawa, Haruo; Tago, Sakie; Umetsu, Kazuteru; Haginiwa, Naomichi; Asao, Naoki
Tetrahedron, 2009 , vol. 65, # 9 p. 1774 - 1784
反应条件
tetra-(n-butyl)ammonium iodide
参考文献
Ochiai, Masahito; Ito, Takao; Takahashi, Hideo; Nakanishi, Akinobu; Toyonari, Mika; Sueda, Takuya; Goto, Satoru; Shiro, Motoo
Journal of the American Chemical Society, 1996 , vol. 118, # 33 p. 7716 - 7730
反应条件
1.1: 4-(N,N-dimethlyamino)pyridine; N-ethyl-N,N-diisopropylamine / dichloromethane / 48 h / 0 - 23 °C / Inert atmosphere
2.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
2.2: 23 °C / Inert atmosphere
View Scheme
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 3 h / 0 °C / Inert atmosphere
2: boron trifluoride diethyl etherate / dichloromethane / 3 h / 0 °C / Inert atmosphere
View Scheme
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 0 - 23 °C / Inert atmosphere
2.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
2.2: 23 °C / Inert atmosphere
View Scheme
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
[Cp*IrCl2(C(NBuCHCHNBu))]; silver trifluoromethanesulfonate
T=110°C; 10 h;
参考文献
Prades, Amparo; Corberan, Rosa; Poyatos, Macarena; Peris, Eduardo
Chemistry - A European Journal, 2008 , vol. 14, # 36 p. 11474 - 11479
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=0°C; 3 h; Inert atmosphere; regioselective reaction;
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=0°C; 3 h; Inert atmosphere; regioselective reaction;
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
1.1: 4-(N,N-dimethlyamino)pyridine; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; dichloromethane / 48 h / 0 - 23 °C / Inert atmosphere
2.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
2.2: 1.5 h / 40 °C / Inert atmosphere
View Scheme
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
