磷酸单(1-甲基乙基)酯合成路线 (共 17 条)
参考文献
Ipatieff; Pines; Friedman
Journal of the American Chemical Society, 1938 , vol. 60, p. 2732
参考文献
Ciba-Geigy Corporation
Patent: US5491261 A1, 1996 ;
反应条件
silver nitrate in acetonitrile
T=0 - 5°C; Hydrolysis; 1 h;
参考文献
Modro, Agnes M.; Modro, Tomasz A.
Organic Preparations and Procedures International, 1992 , vol. 24, # 1 p. 57 - 60
反应条件
phosphorus pentoxide
T=70°C; 10 h; Title compound not separated from byproducts;
参考文献
Munik, S. N.; Eliseenkov, V. N.; Ivanov, B. E.
Russian Journal of General Chemistry, 1995 , vol. 65, # 3.1 p. 378 - 382
Zhurnal Obshchei Khimii, 1995 , vol. 65, # 3 p. 431 - 435
反应条件
sodium cyanide in dimethyl sulfoxide
T=60°C;
参考文献
Thuong,N.T.; Chabrier,P.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1972 , vol. 275, p. 1125 - 1127
反应条件
in water; acetonitrile
Irradiationvar. solvents ratio; pH 2 and pH 7; Quantum yield;
参考文献
Givens, Richard S.; Athey, Phillip S.; Kueper III, L. William; Matuszewski, Bogdan; Xue, Jie-You
Journal of the American Chemical Society, 1992 , vol. 114, # 22 p. 8708 - 8710
反应条件
phosphorus; tetraethylammonium iodide in water; acetonitrile
electrolysis;
参考文献
Romakhin; Nikitin
Russian Journal of General Chemistry, 1998 , vol. 68, # 7 p. 1023 - 1026
反应条件
phosphoric acid
T=50 - 100°C; unter Druck;
参考文献
Ipatieff
Industrial and Engineering Chemistry, 1935 , vol. 27, p. 1068
Z.obsc.Chem., 1936 , vol. 6, p. 331
Full Text Show Details
Ipatieff
Trans.electroch.Soc., 1973 , vol. 71, p. 338
反应条件
water; sodium salt of phosphorous acid
T=100°C;
参考文献
Bailly
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1919 , vol. 168, p. 561
Bulletin de la Societe Chimique de France, 1919 , vol. <4>25, p. 255
Chem. Zentralbl., 1919 , vol. 90, # III p. 254
反应条件
orthophosphorus acid; iodine in ethanol
参考文献
Williams,A.; Naylor,R.A.
Journal of the Chemical Society [Section] B: Physical Organic, 1971 , p. 1973 - 1979