5-氯甲基呋喃-2-甲醛合成路线 （共 59 条）
反应条件
palladium on activated charcoal; hydrogen
参考文献
Mascal, Mark; Nikitin, Edward B.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 41 p. 7924 - 7926
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 41 p. 7924 - 7926
反应条件
in water T=70°C; 1 h; Overall yield = 86 percent;
参考文献
RSC Advances, , vol. 4, # 11 p. 5689 - 5693
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; 1,3-bis(2,4,6-trimethylphenyl)imidazolium chloride in tetrahydrofuran
T=32°C; 3 h;
参考文献
INCITOR INCORPORATED; MIKOCHIK, Peter; CAHANA, Aviad
Patent: WO2012/24353 A1, 2012 ;
Location in patent: Page/Page column 8 ;
反应条件
1: NaN3 / dimethylformamide / 1 h / 65 °C
2: Ph3P / methanol / 2 h / 20 °C
View Scheme
参考文献
Chakraborty, Tushar K; Tapadar, Subhasish; Kiran Kumar
Tetrahedron Letters, 2002 , vol. 43, # 7 p. 1317 - 1320
反应条件
sodium hydroxide
Williamson reaction;
参考文献
Casanova; Iborra; Corma
Journal of Catalysis, 2010 , vol. 275, # 2 p. 236 - 242
反应条件
1: hydrogenchloride / water / |Cooling with ice
2: potassium carbonate / dimethyl sulfoxide / 5 h / 50 °C / |Inert atmosphere
3: hydrogenchloride / water / 2 h
View Scheme
参考文献
Chang, Fei; Dutta, Saikat; Becnel, James J.; Estep, Alden S.; Mascal, Mark
Journal of Agricultural and Food Chemistry, 2014 , vol. 62, # 2 p. 476 - 480
反应条件
1: NaN3 / dimethylformamide / 1 h / 65 °C
View Scheme
参考文献
Chakraborty, Tushar K; Tapadar, Subhasish; Kiran Kumar
Tetrahedron Letters, 2002 , vol. 43, # 7 p. 1317 - 1320
参考文献
DABUR RESEARCH FOUNDATION
Patent: US2005/32707 A1, 2005 ;
Location in patent: Page/Page column 4 ;
