4-TBSMS-羟氧甲基苯硼酸合成路线 （共 4 条）
反应条件
sodium hydroxide; water in tetrahydrofuran T=23°C; 0.166667 h; Inert atmosphere;
参考文献
Gillis, Eric P.; Burke, Martin D.
Journal of the American Chemical Society, 2008 , vol. 130, # 43 p. 14084 - 14085
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; 2: With boric acid trimethyl ester in tetrahydrofuran; hexane T=-78 - 20°C; 17 h; Further stages.;
参考文献
Ashton, Peter R.; Ballardini, Roberto; Balzani, Vincenzo; Credi, Alberto; Dress, Klaus Ruprecht; Ishow, Elena; Kleverlaan, Cornelis J.; Kocian, Oldrich; Preece, Jon A.; Spencer, Neil; Stoddart, J. Fraser; Venturi, Margherita; Wenger, Sabine
Chemistry - A European Journal, 2000 , vol. 6, # 19 p. 3558 - 3574
反应条件
1: 100 percent Chromat. / imidazole / dimethylformamide / 2.5 h / 22 °C 2: n-butyllithium / tetrahydrofuran; toluene; hexane / 2.5 h / -78 °C 3: 1.29 kg / HCl / ethyl acetate; H2O / 1 h / -4 - 3 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 14, # 22 p. 3435 - 3446
反应条件
1: 100 percent Chromat. / imidazole / dimethylformamide / 2.5 h / 22 °C 2: n-butyllithium / tetrahydrofuran; toluene; hexane / 2.5 h / -78 °C 3: 1.29 kg / HCl / ethyl acetate; H2O / 1 h / -4 - 3 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 14, # 22 p. 3435 - 3446
