5-硝基-2-苯基苯并[b]呋喃合成路线 (共 19 条)
反应条件
copper(l) iodide; Na2[PdCl4]; N,N,N',N,-tetramethylethylenediamine; cataCXium PIntB
T=80°C; 5 h; Inert atmosphere;
参考文献
Bochicchio, Antonella; Chiummiento, Lucia; Funicello, Maria; Lopardo, Maria Teresa; Lupattelli, Paolo
Tetrahedron Letters, 2010 , vol. 51, # 21 p. 2824 - 2827
反应条件
1: caesium carbonate / N,N-dimethyl-formamide / 12 h / 110 °C / under air; sealed tube
2: potassium carbonate; palladium dichloride / N,N-dimethyl-formamide / 6 h / 130 °C / under air; sealed tube
View Scheme
参考文献
Wang, Shihua; Li, Pinhua; Yu, Lin; Wang, Lei
Organic Letters, 2011 , vol. 13, # 22 p. 5968 - 5971
反应条件
1: caesium carbonate / N,N-dimethyl-formamide / 12 h / 110 °C / under air; sealed tube
2: potassium carbonate; palladium dichloride / N,N-dimethyl-formamide / 6 h / 130 °C / under air; sealed tube
View Scheme
参考文献
Wang, Shihua; Li, Pinhua; Yu, Lin; Wang, Lei
Organic Letters, 2011 , vol. 13, # 22 p. 5968 - 5971
反应条件
1,10-phenanthroline; Cu(acetate)2*(x)H2O; sodium acetate; palladium diacetate in 1,2-dichloro-ethane
T=110°C; 24 h; Molecular sieve; Kinetics; Reagent/catalystSolventConcentration;
参考文献
Sharma, Upendra; Naveen, Togati; Maji, Arun; Manna, Srimanta; Maiti, Debabrata
Angewandte Chemie - International Edition, 2013 , vol. 52, # 48 p. 12669 - 12673
Angew. Chem., 2013 , vol. 125, # 48 p. 12901 - 12905
反应条件
phosphorus pentoxide; benzene
参考文献
Dilthey; Quint
Journal fuer Praktische Chemie (Leipzig), 1931 , vol. <2> 131, p. 1,26
反应条件
1: ethanol; hydrogen chloride; aqueous perchloric acid
2: acetic acid; aqueous hydrogen peroxide
3: aq. NaOH solution
4: phosphorus (V)-oxide; benzene
View Scheme
参考文献
Dilthey; Quint
Journal fuer Praktische Chemie (Leipzig), 1931 , vol. <2> 131, p. 1,26
反应条件
1: ethanol; hydrogen chloride; aqueous perchloric acid
2: acetic acid; aqueous hydrogen peroxide
3: aq. NaOH solution
4: phosphorus (V)-oxide; benzene
View Scheme
参考文献
Dilthey; Quint
Journal fuer Praktische Chemie (Leipzig), 1931 , vol. <2> 131, p. 1,26
参考文献
Dilthey; Quint
Journal fuer Praktische Chemie (Leipzig), 1931 , vol. <2> 131, p. 1,26
参考文献
Dilthey; Quint
Journal fuer Praktische Chemie (Leipzig), 1931 , vol. <2> 131, p. 1,26