二(二乙基二硫代氨基甲酸)锡(II)盐合成路线 (共 2 条)
反应条件
in water SnCl2*2H2O and Na-salt were dissolved in H2O, stirred for 30 min at roomtemp.; filtered, dried in vacuo;
参考文献
Barone, Giampaolo; Chaplin, Tracy; Hibbert, Thomas G.; Kana, Aliki T.; Mahon, Mary F.; Molloy, Kieran C.; Worsley, Ian D.; Parkin, Ivan P.; Price, Louise S.
Journal of the Chemical Society. Dalton Transactions, 2002 , # 6 p. 1085 - 1092
反应条件
tetrachloromethane; chloroform in water
byproducts: Sn(2+); shaking buffered aq. Hg(2+) soln. (pH=5.6) with Sn((C2H5)2NCSS)2 in CHCl3 or CCl4; fast and complete reaction;;
参考文献
Eckert, F.
Zeitschrift fuer Analytische Chemie, 1957 , vol. 155, p. 23 - 35
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Gmelin Handbook: Hg: MVol.A2, 119, page 873 - 875