2-((2s,3s)-2-((叔丁氧基羰基)氨基)-3-甲基戊酰胺)乙酸甲酯合成路线 （共 4 条）
反应条件
sodium hydrogencarbonate in dichloromethane; water Ambient temperature;
参考文献
Carpino, Louis A.; Mansour, El-Sayed M. E.; Sadat-Aalaee, Dean
Journal of Organic Chemistry, 1991 , vol. 56, # 8 p. 2611 - 2614
反应条件
dicyclohexyl-carbodiimide in acetonitrile T=0°C;
参考文献
Smith, Grant Gill; Evans, Robert C.; Baum, Rocky
Journal of the American Chemical Society, 1986 , vol. 108, # 23 p. 7327 - 7332
反应条件
1: 77.3 percent / cyanuric fluoride, pyridine / CH2Cl2 / 1 h / -10 °C 2: 76.7 percent / NaHCO3 / CH2Cl2; H2O / Ambient temperature View Scheme
参考文献
Carpino, Louis A.; Mansour, El-Sayed M. E.; Sadat-Aalaee, Dean
Journal of Organic Chemistry, 1991 , vol. 56, # 8 p. 2611 - 2614
反应条件
triethylamine in 1,4-dioxane
参考文献
Miroshnikov,A.I. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1970 , vol. 40, # 2 p. 429 - 443,395 - 407
