3,7-二硫杂-1,9-壬二醇合成路线 (共 5 条)
反应条件
1: 2-hydroxyethanethiol With sodium ethanolate in ethanol 2: 1,3-dibromo-propane in ethanol 1 h; Heating;
参考文献
Timperley, Christopher M.; Black, Robin M.; Bird, Michael; Holden, Ian; Mundy, Joanna L.; Read, Robert W.
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 9 p. 2027 - 2046
反应条件
borane-THF in tetrahydrofuran 96 h; Heating;
参考文献
Martinez-Bernhardt, Rolando; Castro, Peter P.; Godjoian, Gayane; Gutierrez, Carlos G.
Tetrahedron, 1998 , vol. 54, # 31 p. 8919 - 8932
反应条件
1: 1,3-dimercaptopropane With sodium ethanolate in ethanol 2: 2-chloro-ethanol in ethanol 1 h; Heating;
参考文献
Timperley, Christopher M.; Black, Robin M.; Bird, Michael; Holden, Ian; Mundy, Joanna L.; Read, Robert W.
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 9 p. 2027 - 2046
反应条件
T=80°C; 4 h; Irradiation;
参考文献
Oswald,A.A. et al.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 1173 - 1184
参考文献
Zhang, Taiping; She, Guangwei; Qi, Xiaopeng; Mu, Lixuan
Tetrahedron, 2013 , vol. 69, # 34 p. 7102 - 7106