4,5,6,7-四氟吲哚合成路线 (共 11 条)
反应条件
potassium hydroxide in acetonitrile 2 h; Reflux;
参考文献
Tetrahedron, , vol. 69, # 39 p. 8477 - 8486
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene 48 h; Heating;
参考文献
Filler, Robert; Chen, Wei; Woods, Sarah M.
Journal of Fluorine Chemistry, 1995 , vol. 73, # 1 p. 95 - 100
反应条件
1: 73 percent / LiAlH4, AlCl3 / diethyl ether / 1 h 2: 61 percent / KF / dimethylformamide / 4 h / Heating 3: 68 percent / DDQ / benzene / 48 h / Heating View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 73, # 1 p. 95 - 100
反应条件
1: 61 percent / KF / dimethylformamide / 4 h / Heating 2: 68 percent / DDQ / benzene / 48 h / Heating View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 73, # 1 p. 95 - 100
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / acetonitrile / 1 h / 50 °C / |Inert atmosphere 2: potassium hydroxide / acetonitrile / 2 h / |Reflux View Scheme
参考文献
Tetrahedron, , vol. 69, # 39 p. 8477 - 8486
反应条件
Yield given. Multistep reaction;
参考文献
Journal of Fluorine Chemistry, , vol. 73, # 1 p. 95 - 100
反应条件
trichlorophosphate in N,N-dimethyl-formamide T=35°C; 3 h;
参考文献
Filler, Robert; Woods, Sarah M.; White, William L.
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1837 - 1841
反应条件
1: 89 percent / phosphorus oxychloride / dimethylformamide / 3 h / 35 °C 2: conc. HCl, amalgamated zinc / aq. ethanol / 0.5 h / Heating View Scheme
参考文献
Filler, Robert; Woods, Sarah M.; White, William L.
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1837 - 1841
反应条件
1: acetic acid / Ambient temperature 2: 99 percent / 24 h 3: 60 percent / sodium cyanide / dimethylformamide / 2 h / Heating View Scheme
参考文献
Filler, Robert; Woods, Sarah M.; White, William L.
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1837 - 1841
反应条件
ethyl bromide; magnesium 1.)THF, reflux, 0.5 h; 2.)THF, reflux, 0.5 h; Yield given. Multistep reaction;
参考文献
Filler, Robert; Woods, Sarah M.; White, William L.
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1837 - 1841