1,1,3,3-四甲基-1,3-二硅代环丁烷合成路线 (共 72 条)
反应条件
T=670°C; Further byproducts given;
参考文献
Conlin,R.T.; Huffaker,H.B.; Kwak,Y.W.
Journal of the American Chemical Society, 1985 , vol. 107, p. 731
参考文献
Auner, N.; Grobe, J.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 2 p. 151 - 178
参考文献
Barton,T.J.; Hussmann,G.P.
Journal of the American Chemical Society, 1985 , vol. 107, p. 7581
反应条件
K/Na; buta-1,3-diene
T=280 - 300°C; P=0.1 - 1 Torr; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Gusel'nikov, L. E.; Polyakov, Yu. P.; Zaikin, V. G.; Nametkin, N. S.
Doklady Chemistry, 1984 , vol. 274, p. 22 - 24
Doklady Akademii Nauk SSSR, 1984 , vol. 274, # 3 p. 598 - 602
反应条件
K/Na
T=280 - 300°C; P=0.1 - 1 Torr; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Gusel'nikov, L. E.; Polyakov, Yu. P.; Zaikin, V. G.; Nametkin, N. S.
Doklady Chemistry, 1984 , vol. 274, p. 22 - 24
Doklady Akademii Nauk SSSR, 1984 , vol. 274, # 3 p. 598 - 602
反应条件
T=760°C; Further byproducts given;
参考文献
Barton,T.J.; Revis,A.; Davidson,I.M.
Journal of the American Chemical Society, 1986 , vol. 108, p. 4022
反应条件
sodium chloride in tetrahydrofuran
Ge-compound in soln. treated with Na2S, stirred (4h, 20°C, Ar); Na2S and NaCl filtered off, distillation under reduced pressure; elem. anal.;
参考文献
Barrau, J.; Hamida, N. Ben; Satge, J.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1990 , vol. 20, p. 1373 - 1386
参考文献
Auner, N.; Grobe, J.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 2 p. 151 - 178
反应条件
in tetrahydrofuran
electrochemical reduction;
参考文献
Bordeau, M.; Biran, C.; Pons, P.; Leger, M.-P.; Dunogues, J.
Journal of Organometallic Chemistry, 1990 , vol. 382, # 3 p. C21 - C24
反应条件
Ambient temperature;
参考文献
Auner, N.; Grobe, J.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 2 p. 151 - 178