1,1,3,3-四甲基-1,3-二硅代环丁烷合成路线 (共 72 条)
反应条件
diethyl ether; magnesium
参考文献
Knoth; Lindsey
Journal of Organic Chemistry, 1958 , vol. 23, p. 1932
参考文献
Auner, N.; Grobe, J.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 2 p. 151 - 178
反应条件
n-butyllithium in diethyl ether; hexane
1) -100 deg C, 2) slow heating; Yield given;
参考文献
Wiberg, Nils; Preiner, Gerhard; Schieda, Oswald
Chemische Berichte, 1981 , vol. 114, # 6 p. 2087 - 2103
反应条件
in benzene
Ar atmosphere; stirring (ambient temp., 10 min); filtration;
参考文献
Barrau, Jacques; Hamida, Najib Ben; Satge, Jacques
Journal of Organometallic Chemistry, 1990 , vol. 387, # 1 p. 65 - 76
参考文献
Kriner,W.A.
Journal of Organic Chemistry, 1964 , vol. 29, p. 1601 - 1606
反应条件
water
T=650 - 720°C; photoionization; Product distribution;
参考文献
Koenig, T.; McKenna, William
Journal of the American Chemical Society, 1981 , vol. 103, # 5 p. 1212 - 1213
参考文献
Barton,T.J.; Revis,A.; Davidson,I.M.
Journal of the American Chemical Society, 1986 , vol. 108, p. 4022
反应条件
potassium-sodium in gaseous matrix
T=280 - 320°C; P=0.1 - 1 Torr; study of reaction of further chloromethylsilanes; Product distributionMechanism;
参考文献
Gusel'nikov, L. E.; Polyakov, Yu. P.; Volnina, E. A.; Nametkin, N. S.
Journal of Organometallic Chemistry, 1985 , vol. 292, p. 189 - 204
反应条件
in benzene
Ar atmosphere; stirring (ambient temp., 10 min); filtration;
参考文献
Barrau, Jacques; Hamida, Najib Ben; Satge, Jacques
Journal of Organometallic Chemistry, 1990 , vol. 387, # 1 p. 65 - 76
参考文献
Barton,T.J.; Wulff,W.D.
Journal of Organometallic Chemistry, 1979 , vol. 168, p. 23 - 31