1,1,3,3-四甲基-1,3-二硅代环丁烷合成路线 (共 72 条)
反应条件
potassium
T=300°C; P=0.1 Torr; gas-phase reaction, other reagent: Na; Mechanism;
参考文献
Gusel'nikov, L.E.; Polyakov, Yu.P.; Volnina, E.A.; Ivanov, A.V.; Nametkin, N.S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 11 p. 2425 - 2426
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 11 p. 2645 - 2646
反应条件
1.) argonmatrix, 10 K, irradiation, 2.) argonmatrix, 35 K;
参考文献
Trommer, Martin; Sander, Wolfram; Ottosson, Carl-Henrik; Cremer, Dieter
Angewandte Chemie, 1995 , vol. 107, # 8 p. 999 - 1001
反应条件
oxygen
T=519.9°C; P=0.6 Torr; Ea; Rate constantThermodynamic dataMechanism;
参考文献
Davidson, Iain M. T.; Dean, Christopher E.; Lawrence, F. Timothy
Journal of the Chemical Society, Chemical Communications, 1981 , # 2 p. 52 - 53
反应条件
T=700 - 750°C; P=0.0001 - 0.1 Torr; other monosilacyclobutanes, also deuterated, var. temp.; Mechanism;
参考文献
Nefedov, O. M.; Maltsev, A. K.; Khabashesku, V. N.; Korolev, V. A.
Journal of Organometallic Chemistry, 1980 , vol. 201, # 1 p. 123 - 136
反应条件
1.) argonmatrix, 10 K, irradiation, 2.) argonmatrix, 30 K - 35 K; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Trommer, Martin; Sander, Wolfram; Ottosson, Carl-Henrik; Cremer, Dieter
Angewandte Chemie, 1995 , vol. 107, # 8 p. 999 - 1001
反应条件
T=680°C; other temperatures; Product distribution;
参考文献
Hassner, Alfred; Soderquist, John A.
Tetrahedron Letters, 1980 , vol. 21, p. 429 - 432
反应条件
argon
T=399.9°C; 0.166667 h; IrradiationEa, ΔH, ΔS, var. temp.; MechanismThermodynamic dataProduct distribution;
参考文献
Davidson; Potzinger; Reimann
Berichte der Bunsengesellschaft/Physical Chemistry Chemical Physics, 1982 , vol. 86, # 1 p. 13 - 19
反应条件
T=550°C; other temperatures; Product distribution;
参考文献
Hassner, Alfred; Soderquist, John A.
Tetrahedron Letters, 1980 , vol. 21, p. 429 - 432
反应条件
hydrogen bromide
HeatingEa; Rate constantThermodynamic data;
参考文献
Davidson, Iain M. T.; Dean, Christopher E.; Lawrence, F. Timothy
Journal of the Chemical Society, Chemical Communications, 1981 , # 2 p. 52 - 53
反应条件
T=45 - 55°C; 3 h; Product distribution;
参考文献
Gazizov, T. Kh.; Ustanova, L. N.; Ryzhikov, D. V.; Pudovik, A. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1673 - 1674
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1830 - 1832