1,1,3,3-四甲基-1,3-二硅代环丁烷合成路线 (共 72 条)
反应条件
in absence of light at -78°C (3 h) then at 20°C (24 h);
参考文献
Gmelin Handbook: F: PerFHalOrg.8, 4, page 152 - 228
反应条件
5 h; Ambient temperature; Further byproducts given;
参考文献
Ducker, Graham E.; Tipping, Anthony E.
Journal of Fluorine Chemistry, 1994 , vol. 67, # 2 p. 129 - 136
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Devine,A.M. et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1975 , p. 1434 - 1439
反应条件
zirconium tetrachloride in benzene
T=20°C; 22 h; Product distribution;
参考文献
Vdovin, V. M.; Bespalova, N. B.; Sergeeva, M. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, p. 1768 - 1769
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 8 p. 1917 - 1919
反应条件
tungsten
P=5E-06 Torr; Gas phaseHeating; Activation energy;
参考文献
Tong; Shi
Journal of Mass Spectrometry, 2010 , vol. 45, # 2 p. 215 - 222
反应条件
platinum(II) acetylacetonate in dichloromethane
Addition; hydrosilylation; 8 h; UV-irradiation; Further byproducts given;
参考文献
Wu, Xiaosong; Malpert, John H.; Zang, Hongmei; Neckers, Douglas C.
Tetrahedron Letters, 1999 , vol. 40, # 48 p. 8309 - 8312
反应条件
platinum(II) acetylacetonate in dichloromethane
Addition; hydrosilylation; 2 h; UV-irradiation;
参考文献
Wu, Xiaosong; Malpert, John H.; Zang, Hongmei; Neckers, Douglas C.
Tetrahedron Letters, 1999 , vol. 40, # 48 p. 8309 - 8312
反应条件
platinum(II) acetylacetonate in dichloromethane
Addition; hydrosilylation; 2 h; UV-irradiation;
参考文献
Wu, Xiaosong; Malpert, John H.; Zang, Hongmei; Neckers, Douglas C.
Tetrahedron Letters, 1999 , vol. 40, # 48 p. 8309 - 8312
参考文献
Kriner,W.A.
Journal of Organometallic Chemistry, 1977 , vol. 134, p. 15 - 20
反应条件
-78 to 25°C; elem. anal.;
参考文献
Auner, N.; Grobe, J.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1983 , vol. 500, p. 132 - 160