3,4-二氢-2,2-二甲基-2H-萘并[1,2-b]吡喃合成路线 （共 18 条）
反应条件
phosphoric acid in Petroleum ether
T=30 - 35°C; 0.5 h;
参考文献
Ahluwalia, V. K.; Hira, P. K.; Jolly, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 10 p. 961 - 962
反应条件
3,4,5,6-tetrachloro-1,2-benzoquinone; [Mo(CO)3(cyclopentadienyl)Cl] in chlorobenzene
T=150°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Yamamoto, Yoshihiko; Itonaga, Kouhei
Organic Letters, 2009 , vol. 11, # 3 p. 717 - 720
反应条件
zeolite HSZ-360 in chlorobenzene
T=120°C; 6 h;
参考文献
Bigi, Franca; Carloni, Silvia; Maggi, Raimondo; Muchetti, Chiara; Rastelli, Massimo; Sartori, Giovanni
Synthesis, 1998 , # 3 p. 301 - 304
反应条件
CuAl-SBA-15 in cyclohexane
T=85°C; 6 h;
参考文献
Varghese, Shaji; Anand, Chokkalinkam; Dhawale, Dattatray; Mano, Ajayan; Balasubramanian, Veerappan V.; Raj, George Allen Gnana; Nagarajan, Samuthira; Wahab, Mohammad A.; Vinu, Ajayan
Tetrahedron Letters, 2012 , vol. 53, # 42 p. 5656 - 5659
反应条件
in chloroform
T=60°C;
参考文献
Renzi, Augusto De; Lombardi, Angelina; Panunzi, Achille; Saporito, Antonio
Gazzetta Chimica Italiana, 1988 , vol. 118, # 9 p. 657 - 660
反应条件
1: 98 percent / phenylboronic acid / acetic acid; toluene / 4 h / Heating
2: 100 percent / H2 / 10 percent Pd/C / ethyl acetate / 1 h / 2068.59 Torr
View Scheme
参考文献
Alves, Glaucia B. C.; Lopes, Rosangela S. C.; Lopes, Claudio C.; Snieckus, Victor
Synthesis, 1999 , # 11 p. 1875 - 1877
反应条件
1: 98 percent / phenylboronic acid / acetic acid; toluene / 4 h / Heating
2: 100 percent / H2 / 10 percent Pd/C / ethyl acetate / 1 h / 2068.59 Torr
View Scheme
参考文献
Alves, Glaucia B. C.; Lopes, Rosangela S. C.; Lopes, Claudio C.; Snieckus, Victor
Synthesis, 1999 , # 11 p. 1875 - 1877
反应条件
1: 84 percent / formic acid, conc. hydrochloric acid / 1 h / 110 °C
2: 82 percent / lithium aluminium hydride / tetrahydrofuran / 0.5 h / Heating
3: 6 N aq. HCl / tetrahydrofuran
4: 100 percent / H2 / 10percent palladium on carbon / tetrahydrofuran / 0.25 h
View Scheme
参考文献
Amaral; Barnes
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 6 p. 1457 - 1460
反应条件
1: 6 N aq. HCl / tetrahydrofuran
2: 100 percent / H2 / 10percent palladium on carbon / tetrahydrofuran / 0.25 h
View Scheme
参考文献
Amaral; Barnes
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 6 p. 1457 - 1460
反应条件
1: 4.3 g / 85 percent orthophosphoric acid / xylene / 8 h
2: 3.1 g / 85 percent HCOOH / 4 h / 60 °C
View Scheme
参考文献
Chiou, Wen-Fei; Li, Shyh-Yuan; Ho, Li-Kang; Hsien, Ming-Ling; Don, Ming-Jaw
European Journal of Medicinal Chemistry, 2002 , vol. 37, # 1 p. 69 - 75
