甲基吩噻嗪-10-基甲酮合成路线 （共 28 条）
反应条件
in toluene T=50°C; 1 h;
参考文献
Auvin, Serge; Chabrier De Lassauniere, Pierre-Etienne
Patent: US2005/222045 A1, 2005 ;
Location in patent: Page/Page column 13 ;
反应条件
phosphoric acid T=60°C; 0.166667 h; Microwave irradiation; regioselective reaction;
参考文献
Gaina, Luiza; Porumb, Dan; Silaghi-Dumitrescu, Ioan; Cristea, Castelia; Silaghi-Dumitrescu, Luminita
Canadian Journal of Chemistry, 2010 , vol. 88, # 1 p. 42 - 49
反应条件
N-bromosuccinmide in chloroform 0.5 h; Ambient temperature;
参考文献
Caputo, Romualdo; Ferreri, Carla; Longobardo, Luigi; Mastroianni, Domenico; Palumbo, Giovanni; Pedatella, Silvana
Heterocycles, 1993 , vol. 36, # 7 p. 1641 - 1644
反应条件
carbon disulfide; aluminium trichloride
参考文献
Baltzly et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 2673,2677
反应条件
1: hydrazine hydrate / ethanol / 18 h / |Reflux 2: ethanol / 24 h / |Reflux View Scheme
参考文献
Baciu-Atudosie, Lavinia; Ghinet, Alina; Belei, Dalila; Gautret, Philippe; Rigo, Benoit; Bicu, Elena
Tetrahedron Letters, 2012 , vol. 53, # 45 p. 6127 - 6131
参考文献
Bernthsen
Justus Liebigs Annalen der Chemie, 1885 , vol. 230, p. 169,170
Chemische Berichte, 1906 , vol. 39, p. 1808
反应条件
1: AlCl3; CS2 2: aqueous NaClO View Scheme
参考文献
Massie et al.
Journal of Organic Chemistry, 1956 , vol. 21, p. 1006
反应条件
(i) AlCl3, CS2, (ii) aq. HCl; Multistep reaction;
参考文献
Takada,A.; Nishimura,H.
Chemical and Pharmaceutical Bulletin, 1962 , vol. 10, p. 1 - 8
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran 24 h; Ambient temperature;
参考文献
Babudri, F.; Ciminale, F.; Nunno, L. Di; Florio, S.
Tetrahedron, 1982 , vol. 38, # 4 p. 557 - 561
反应条件
1: AlCl3 / CS2 / 6 h / Heating 2: aq. HCl / ethanol View Scheme
参考文献
Cauquil; Casadevall
Bulletin de la Societe Chimique de France, 1955 , p. 768,781
