甲基吩噻嗪-10-基甲酮合成路线 （共 28 条）
反应条件
carbon disulfide; aluminium trichloride Erwaermen des Reaktionsprodukts mit wss. HCl;
参考文献
Baltzly et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 2673,2677
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Massie et al.
Journal of Organic Chemistry, 1956 , vol. 21, p. 1006
反应条件
(i) AlCl3, CS2, (ii) aq. HCl; Multistep reaction;
参考文献
Takada,A.; Nishimura,H.
Chemical and Pharmaceutical Bulletin, 1962 , vol. 10, p. 1 - 8
反应条件
(i) AlCl3, CS2, (ii) KOH, EtOH; Multistep reaction;
参考文献
Gritsenko,A.N.; Zhuravlev,S.V.
J. Gen. Chem. USSR (Engl. Transl.), 1960 , vol. 30, p. 2640 - 2645,2622 - 2626
反应条件
1: AlCl3 / CS2 / 6 h / Heating 2: aq. HCl / ethanol 3: NaH View Scheme
参考文献
Chan, Cecil; Yin, Hong; Garforth, Jacqui; McKie, James H.; Jaouhari, Rabih; Speers, Peter; Douglas, Kenneth T.; Rock, Peter J.; Yardley, Vanessa; Croft, Simon L.; Fairlamb, Alan H.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 2 p. 148 - 156
反应条件
N,N,N',N,-tetramethylethylenediamine; dimethylsulfide borane complex; boron trifluoride diethyl etherate 1.) THF, 0.25 h, 2.) ether, 30 min; Yield given. Multistep reaction;
参考文献
Brown, Herbert C.; Narasimhan, S.; Choi, Yong Moon
Synthesis, 1981 , # 12 p. 996 - 997
反应条件
1: aqueous H2O2; acetic acid
2: aq.-ethanolic KOH
View Scheme
参考文献
Toei
Nippon Kagaku Zasshi, 1956 , vol. 77, p. 1270
Chem.Abstr., 1958 , p. 961
反应条件
carbon disulfide; aluminium trichloride
参考文献
Chan, Cecil; Yin, Hong; Garforth, Jacqui; McKie, James H.; Jaouhari, Rabih; Speers, Peter; Douglas, Kenneth T.; Rock, Peter J.; Yardley, Vanessa; Croft, Simon L.; Fairlamb, Alan H.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 2 p. 148 - 156
反应条件
carbon disulfide; aluminium trichloride
参考文献
Cauquil; Casadevall
Bulletin de la Societe Chimique de France, 1955 , p. 768,781
反应条件
1: With AlCl3, aluminium chloride in carbon disulfide
T=55°C; 2 h;
2: With water
参考文献
Auvin, Serge; Chabrier De Lassauniere, Pierre-Etienne
Patent: US2005/222045 A1, 2005 ;
Location in patent: Page/Page column 13 ;
反应条件
carbon disulfide; aluminium trichloride
Behandeln des Reaktionsprodukts mit aethanol. HCl;
参考文献
Massie et al.
Journal of Organic Chemistry, 1956 , vol. 21, p. 1006
