tri-tert-butyl phosphine; caesium carbonate; bis(.eta.(2)-ethylene)(2,4,-pentanedionato)rhodium in 1,4-dioxane T=100°C; Title compound not separated from byproducts;
参考文献
Matsuda, Takanori; Makino, Masaomi; Murakami, Masahiro
Bulletin of the Chemical Society of Japan, 2005 , vol. 78, # 8 p. 1528 - 1533
in tetrahydrofuran T=60°C; 6 h; Inert atmosphereFlow reactor;
参考文献
Murray, Philip R. D.; Browne, Duncan L.; Pastre, Julio C.; Butters, Chris; Guthrie, Duncan; Ley, Steven V.
Organic Process Research and Development, 2013 , vol. 17, # 9 p. 1192 - 1208