2-异丙基-2-苯基环氧乙烷合成路线 (共 3 条)
反应条件
[Pd2H2(1,3-bis(diphenylphosphino)propane)3](TfO)2 in tetrahydrofuran
T=100°C; 24 h; Schlenk techniqueInert atmosphereGlovebox;
参考文献
Mazet, Clement
Chimia, 2013 , vol. 67, # 9 p. 658 - 662
反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '3556712', constants.ctx, '0')">potassium <i>tert</i>-butylate</a> <b>in</b> neat (no solvent)<br />T=70°C; 1 h; kugelrohr distillation at the end of reaction; <br />
参考文献
Toda, Fumio; Kanemoto, Kazuyuki Heterocycles, 1997 , vol. 46, # 1 p. 185 - 188
反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '3556712', constants.ctx, '0')">potassium <i>tert</i>-butylate</a> <b>in</b> neat (no solvent)<br />T=50°C; 3 h; <br />
参考文献
Toda, Fumio; Kanemoto, Kazuyuki Heterocycles, 1997 , vol. 46, # 1 p. 185 - 188