(2,6-二甲基苯氧基)(三甲基)硅烷合成路线 （共 8 条）
反应条件
Lanthanum chloride in dichloromethane
T=20°C; 3.5 h;
参考文献
Narsaiah, Akkirala Venkat
Journal of Organometallic Chemistry, 2007 , vol. 692, # 17 p. 3614 - 3618
反应条件
Nafion-H in tetrachloromethane
1 h; Heating;
参考文献
Olah, George A.; Husain, Altaf; Singh, Brij P.
Synthesis, 1983 , # 11 p. 892 - 895
反应条件
in tetrahydrofuran
1 h; Inert atmosphere;
参考文献
Kindra, Douglas R.; Casely, Ian J.; Fieser, Megan E.; Ziller, Joseph W.; Furche, Filipp; Evans, William J.
Journal of the American Chemical Society, 2013 , vol. 135, # 20 p. 7777 - 7787
反应条件
in tetrahydrofuran
1 h; Inert atmosphere;
参考文献
Kindra, Douglas R.; Casely, Ian J.; Fieser, Megan E.; Ziller, Joseph W.; Furche, Filipp; Evans, William J.
Journal of the American Chemical Society, 2013 , vol. 135, # 20 p. 7777 - 7787
反应条件
tetrahydrofuran; diethyl ether
参考文献
Wilson et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 1717
反应条件
n-butyllithium
1.) hexane, THF, RT, 1 h, 2.) THF, hexane, RT, 1 h; Yield given. Multistep reaction;
参考文献
Kanehisa, Nobuko; Kai, Yasushi; Kasai, Nobutami; Yasuda, Hajime; Nakayama, Yuushou; Nakamura, Akira
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 5 p. 1197 - 1201
反应条件
triphenylphosphine; diethylazodicarboxylate
1) THF, -78 deg C, 10 min, 2) to r.t., overnight; Yield given. Multistep reaction;
参考文献
Clive; Kellner
Tetrahedron Letters, 1991 , vol. 32, # 49 p. 7159 - 7160
参考文献
White,D.M.
Journal of Organic Chemistry, 1969 , vol. 34, p. 297 - 303
