2-(4-氟苯基)-苯并噻唑合成路线 （共 35 条）
反应条件
palladium 10 on activated carbon in N-dodecane; N,N-dimethyl acetamide
T=120°C; 13 h; Inert atmosphere;
参考文献
Jin, Xukang; Liu, Yuxiao; Lu, Qiongqiong; Yang, Dejun; Sun, Jiangkai; Qin, Shuangshuang; Zhang, Jingwu; Shen, Jiaxuan; Chu, Changhu; Liu, Renhua
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 23 p. 3776 - 3780
反应条件
1-methyl-pyrrolidin-2-one
T=100°C; Jacobson's cyclization; 4 h;
参考文献
Chen, Lianqing; Yang, Chuluo; Li, Suyue; Qin, Jingui
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2007 , vol. 68, # 2 p. 317 - 322
反应条件
dipotassium peroxodisulfate; FeCl3·6H2O in water; dimethyl sulfoxide
T=100°C; 12 h; Overall yield = 63 percent;
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
反应条件
potassium carbonate; tris(dibenzylideneacetone)dipalladium (0) in ethylene glycol dimethyl ether; water
T=100°C; Suzuki biaryl coupling; 6 h;
参考文献
Majo, Vattoly J.; Prabhakaran, Jaya; Mann, J. John; Kumar, J. S. Dileep
Tetrahedron Letters, 2003 , vol. 44, # 47 p. 8535 - 8537
反应条件
(R)-(+)-1,1'-binaphthyl-2,2'-diamine; caesium carbonate; copper dichloride in acetonitrile
T=110°C; 36 h; Inert atmosphere;
参考文献
Jaseer; Prasad; Dandapat, Arpan; Sekar, Govindasamy
Tetrahedron Letters, 2010 , vol. 51, # 38 p. 5009 - 5012
反应条件
sodium dithionite in dimethyl sulfoxide
T=80°C; 4 h; Molecular sieve;
参考文献
Wang, Zhanglin; Tang, Riyuan; Xiao, Qin
Chinese Journal of Chemistry, 2011 , vol. 29, # 2 p. 314 - 320
反应条件
iron sulphate heptahydrate; oxygen in diethylene glycol dimethyl ether; water
T=150°C; 20 h; Sealed tube;
参考文献
Liu, Saiwen; Chen, Ru; Guo, Xiangyu; Yang, Huiqiong; Deng, Guojun; Li, Chao-Jun
Green Chemistry, 2012 , vol. 14, # 6 p. 1577 - 1580
反应条件
1: With copper diacetate; potassium ethylxanthate in N,N-dimethyl-formamide
T=80°C; 15 h; Inert atmosphere;
2: With hydrogenchloride in N,N-dimethyl-formamide
T=20°C; 8 h;
参考文献
Prasad; Sekar
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 10 p. 1659 - 1665
反应条件
manganese triacetate in acetic acid
T=110°C; 0.1 h; microwave irradiation;
参考文献
Mu, Xue-Jun; Zou, Jian-Ping; Zeng, Run-Sheng; Wu, Jun-Chen
Tetrahedron Letters, 2005 , vol. 46, # 25 p. 4345 - 4347
反应条件
palladium diacetate; copper (II) acetate monohydrate in 1-methyl-pyrrolidin-2-one; diethylene glycol dimethyl ether
T=120°C; 24 h; sealed vessel;
参考文献
Chen, Ru; Liu, Saiwen; Liu, Xinhua; Yang, Luo; Deng, Guo-Jun
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 22 p. 7675 - 7679
