2-(4-氟苯基)-苯并噻唑合成路线 (共 35 条)
反应条件
1,10-phenanthroline; CuCl2·2H2O; potassium carbonate; sulfur in water
T=100°C; 24 h;
参考文献
Deng, Hang; Li, Zhengkai; Ke, Fang; Zhou, Xiangge
Chemistry - A European Journal, 2012 , vol. 18, # 16 p. 4840 - 4843
反应条件
potassium fluoride; C94H134O4P2Pd2; silver fluoride in cyclohexane
T=90°C; 14 h; Sealed tube;
参考文献
Lee, Hong Geun; Milner, Phillip J.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2014 , vol. 136, # 10 p. 3792 - 3795
反应条件
(R)-(+)-1,1'-binaphthyl-2,2'-diamine; caesium carbonate; copper dichloride in acetonitrile
T=82°C; 96 h; Inert atmosphere;
参考文献
Jaseer; Prasad; Dandapat, Arpan; Sekar, Govindasamy
Tetrahedron Letters, 2010 , vol. 51, # 38 p. 5009 - 5012
反应条件
copper(l) iodide; 1,10-phenanthroline; Na2S*9H2O in acetic acid
T=100°C; 12 h; Sealed tube;
参考文献
Liu, Jidan; Gui, Qingwen; Yang, Zhiyong; Tan, Ze; Guo, Ruqing; Shi, Ji-Cheng
Synthesis (Germany), 2013 , vol. 45, # 7 art. no. SS-2012-F0968-OP, p. 943 - 951
反应条件
[2,2']bipyridinyl; [Ni(O2CCH3)2]*4H2O; lithium tert-butylate in 1,4-dioxane
T=120°C; 36 h; Inert atmosphere;
参考文献
Yamamoto, Takuya; Muto, Kei; Komiyama, Masato; Canivet, Jerome; Yamaguchi, Junichiro; Itami, Kenichiro
Chemistry - A European Journal, 2011 , vol. 17, # 36 p. 10113 - 10122
反应条件
1: in water; dimethyl sulfoxide
T=100°C; 1 h; Inert atmosphere;
2: With dipotassium peroxodisulfate
3 h; Inert atmosphere;
参考文献
Yang, Zhiyong; Chen, Xiang; Wang, Sizhuo; Liu, Jidan; Xie, Kai; Wang, Anwei; Tan, Ze
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 7086 - 7091
反应条件
toluene-4-sulfonic acid
T=118 - 120°C; 0.025 h; microwave irradiation;
参考文献
Paul, Satya; Gupta, Mukta; Gupta, Rajive
Synthetic Communications, 2002 , vol. 32, # 23 p. 3541 - 3547
反应条件
1: 60 percent / CBr4; n-BuLi
2: 48 percent / aq. K2CO3 / Pd2(dba)3 / 1,2-dimethoxy-ethane; H2O / 6 h / 100 °C
View Scheme
参考文献
Majo, Vattoly J.; Prabhakaran, Jaya; Mann, J. John; Kumar, J. S. Dileep
Tetrahedron Letters, 2003 , vol. 44, # 47 p. 8535 - 8537
反应条件
D-glucopyranose; oxygen; glucose oxidase; chloroperoxidase
pH=6; 12 h; Citrate bufferEnzymatic reaction;
参考文献
Kumar, Atul; Sharma, Siddharth; Maurya, Ram Awatar
Tetrahedron Letters, 2010 , vol. 51, # 48 p. 6224 - 6226
反应条件
T=200°C; 0.166667 h; Irradiationmicrowave;
参考文献
Kamila, Sukanta; Koh, Benjamin; Biehl, Edward R.
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 6 p. 1609 - 1612