2-(4-氟苯基)-苯并噻唑合成路线 （共 35 条）
反应条件
1.1: tetrahydrofuran / 12 h / 20 °C
2.1: potassium ethylxanthate; copper diacetate / N,N-dimethyl-formamide / 15 h / 80 °C / |Inert atmosphere
2.2: 8 h / 20 °C
View Scheme
参考文献
Prasad; Sekar
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 10 p. 1659 - 1665
反应条件
1: CuCl2·2H2O; 1,10-phenanthroline; potassium carbonate; sulfur / water / 24 h / 100 °C
2: CuCl2·2H2O; 1,10-phenanthroline; potassium carbonate; sulfur / water / 24 h / 100 °C
View Scheme
参考文献
Deng, Hang; Li, Zhengkai; Ke, Fang; Zhou, Xiangge
Chemistry - A European Journal, 2012 , vol. 18, # 16 p. 4840 - 4843
反应条件
1: isopentyl nitrite / tetrahydrofuran / 0.5 h / |Reflux
2: FeCl3·6H2O; dipotassium peroxodisulfate / dimethyl sulfoxide; water / 12 h / 100 °C
View Scheme
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
反应条件
1: isopentyl nitrite / tetrahydrofuran / 0.5 h / |Reflux
2: FeCl3·6H2O; dipotassium peroxodisulfate / dimethyl sulfoxide; water / 12 h / 100 °C
View Scheme
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
反应条件
1: SOCl2
2: 93 percent / N-methyl-pyrrolidinone / 4 h / 100 °C
View Scheme
参考文献
Chen, Lianqing; Yang, Chuluo; Li, Suyue; Qin, Jingui
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2007 , vol. 68, # 2 p. 317 - 322
