5,7-二甲氧基-4'-羟基黄酮合成路线 （共 8 条）
反应条件
hydrogen; palladium on activated charcoal in methanol; ethyl acetate T=25°C; 3 h;
参考文献
Lin, An-Shen; Nakagawa-Goto, Kyoko; Chang, Fang-Rong; Yu, Donglei; Morris-Natschke, Susan L.; Wu, Chin-Chung; Chen, Shu-Li; Wu, Yang-Chang; Lee, Kuo-Hsiung
Journal of Medicinal Chemistry, 2007 , vol. 50, # 16 p. 3921 - 3927
反应条件
1: 79 percent / aq. KOH / ethanol / 30 h / 20 °C 2: 74 percent / iodine; pyridine / 3 h / Heating 3: 83 percent / H2 / Pd/C / methanol; ethyl acetate / 3 h / 25 °C View Scheme
参考文献
Lin, An-Shen; Nakagawa-Goto, Kyoko; Chang, Fang-Rong; Yu, Donglei; Morris-Natschke, Susan L.; Wu, Chin-Chung; Chen, Shu-Li; Wu, Yang-Chang; Lee, Kuo-Hsiung
Journal of Medicinal Chemistry, 2007 , vol. 50, # 16 p. 3921 - 3927
反应条件
1: 79 percent / aq. KOH / ethanol / 30 h / 20 °C 2: 74 percent / iodine; pyridine / 3 h / Heating 3: 83 percent / H2 / Pd/C / methanol; ethyl acetate / 3 h / 25 °C View Scheme
参考文献
Lin, An-Shen; Nakagawa-Goto, Kyoko; Chang, Fang-Rong; Yu, Donglei; Morris-Natschke, Susan L.; Wu, Chin-Chung; Chen, Shu-Li; Wu, Yang-Chang; Lee, Kuo-Hsiung
Journal of Medicinal Chemistry, 2007 , vol. 50, # 16 p. 3921 - 3927
反应条件
1: 74 percent / iodine; pyridine / 3 h / Heating 2: 83 percent / H2 / Pd/C / methanol; ethyl acetate / 3 h / 25 °C View Scheme
参考文献
Lin, An-Shen; Nakagawa-Goto, Kyoko; Chang, Fang-Rong; Yu, Donglei; Morris-Natschke, Susan L.; Wu, Chin-Chung; Chen, Shu-Li; Wu, Yang-Chang; Lee, Kuo-Hsiung
Journal of Medicinal Chemistry, 2007 , vol. 50, # 16 p. 3921 - 3927
反应条件
hydrogenchloride; sodium nitrite Anschliessend Erwaermen mit wss. Schwefelsaeure;
参考文献
Anand; Venkataraman
Proceedings - Indian Academy of Sciences, Section A, 1947 , # 26 p. 279,282
反应条件
1: iron-powder; acetic acid 2: aqueous hydrochloric acid; sodium nitrite / Anschliessend Erwaermen mit wss. Schwefelsaeure View Scheme
参考文献
Anand; Venkataraman
Proceedings - Indian Academy of Sciences, Section A, 1947 , # 26 p. 279,282
反应条件
1: concentrated sulfuric acid 2: iron-powder; acetic acid 3: aqueous hydrochloric acid; sodium nitrite / Anschliessend Erwaermen mit wss. Schwefelsaeure View Scheme
参考文献
Anand; Venkataraman
Proceedings - Indian Academy of Sciences, Section A, 1947 , # 26 p. 279,282
反应条件
aluminium trichloride; nitrobenzene
参考文献
Anand; Venkataraman
Proceedings - Indian Academy of Sciences, Section A, 1947 , # 26 p. 279,282
Full Text Show Details
Mahal; Venkataraman
Journal of the Chemical Society, 1936 , p. 569
