(S)-(-)-2-(Boc-氨基)-1,5-戊二醇合成路线 （共 13 条）
反应条件
1: 99.3 percent / SOCl2 / 0.5 h / Heating 2: 68.7 percent / DMAP / acetonitrile / 24 h 3: 73.9 percent / NaBH4 / 1,2-dimethoxy-ethane; methanol / 36 h / 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 31, # 5 p. 697 - 706
反应条件
1: Et3N / CH2Cl2 / 1 h / -10 - 0 °C 2: aq. NH4OH / acetonitrile / 48 h / Ambient temperature View Scheme
参考文献
Moon, Sung-Hwan; Lee, Sujin
Synthetic Communications, 1998 , vol. 28, # 21 p. 3919 - 3926
反应条件
1: triphenylphosphine; di-isopropyl azodicarboxylate / dichloromethane / 48 h / 20 °C 2: hydrogenchloride / methanol / 20 °C View Scheme
参考文献
Savage, Scott; Babu, Srinivasan; Zak, Mark; Mao, Zhongping; Cao, Jianhua; Ge, Yonghui; Ma, Dongxu; Jiang, Guoqiang
Synlett, 2013 , vol. 24, # 8 art. no. ST-2013-R0106-L, p. 987 - 990
