6-甲基-4-苯基香豆素合成路线 （共 47 条）
反应条件
triethylamine in chloroform 0.5 h; Heating;
参考文献
Natarajan, M.; Manimaran, T.; Ramakrishnan, V. T.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 6 p. 529 - 534
反应条件
1.1: triphenylphosphine; lithium hydroxide hydrate; lithium chloride / water / |Reflux 2.1: calcium carbonate; palladium diacetate / methanol / 4 h / 60 °C 2.2: 20 °C View Scheme
参考文献
Organic Letters, , vol. 14, # 23 p. 6036 - 6039
反应条件
1: AlCl3 / 130 - 140 °C 3: zinc; benzene / Behandeln des Reaktionsprodukts mit Thionylchlorid und Pyridin 4: aqueous hydriodic acid View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 21, p. 109
反应条件
1: triethylamine 2: 58 percent / Pd(PPh3)4; Cs2CO3 / toluene; H2O / 12 h / 80 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 47, # 10 p. 1525 - 1528
反应条件
1: 74 percent / pyridine / benzene / 3 h 2: 63 percent / conc. sulphuric acid / 0.25 h / 95 °C 3: 69 percent / triethylamine / CHCl3 / 0.5 h / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 23, # 6 p. 529 - 534
反应条件
1: thionyl chloride / Heating 2: 74 percent / pyridine / benzene / 3 h 3: 63 percent / conc. sulphuric acid / 0.25 h / 95 °C 4: 69 percent / triethylamine / CHCl3 / 0.5 h / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 23, # 6 p. 529 - 534
反应条件
1: 63 percent / conc. sulphuric acid / 0.25 h / 95 °C 2: 69 percent / triethylamine / CHCl3 / 0.5 h / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 23, # 6 p. 529 - 534
反应条件
1.1: n-butyllithium / diethyl ether; hexane / 0.5 h / 0 °C / |Reflux; |Inert atmosphere 1.2: 0 - 20 °C 2.1: iodine / toluene / 5 h / |Reflux; |Inert atmosphere 3.1: palladium diacetate; caesium carbonate / diethylene glycol dimethyl ether / 12 h / 100 °C / 760.05 Torr / |Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 30 p. 10954 - 10957
反应条件
1: iodine / toluene / 5 h / |Reflux; |Inert atmosphere 2: palladium diacetate; caesium carbonate / diethylene glycol dimethyl ether / 12 h / 100 °C / 760.05 Torr / |Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 30 p. 10954 - 10957
反应条件
1.1: n-butyllithium / diethyl ether; hexane / 0.5 h / 0 °C / |Reflux; |Inert atmosphere 1.2: 0 - 20 °C 2.1: iodine / toluene / 5 h / |Reflux; |Inert atmosphere 3.1: palladium diacetate; caesium carbonate / diethylene glycol dimethyl ether / 12 h / 100 °C / 760.05 Torr / |Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 30 p. 10954 - 10957
