6-甲基-4-苯基香豆素合成路线 (共 47 条)
反应条件
1: aluminium chloride; carbon disulfide 2: sulfur / 200 °C View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 573,577, 582
参考文献
Journal of the Chemical Society, , p. 1180,1182
反应条件
1: magnesium; benzene 2: hydrogen fluoride View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 587, p. 1,15
反应条件
2: zinc; benzene / Behandeln des Reaktionsprodukts mit Thionylchlorid und Pyridin 3: aqueous hydriodic acid View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 21, p. 109
反应条件
1: zinc; benzene / Behandeln des Reaktionsprodukts mit Thionylchlorid und Pyridin 2: aqueous hydriodic acid View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 21, p. 109
参考文献
Justus Liebigs Annalen der Chemie, , vol. 587, p. 1,15
参考文献
Journal of the Indian Chemical Society, , vol. 21, p. 109
反应条件
1: With sodium hydroxide; hydrogen; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in methanol T=50°C; P=9000.9 Torr; 24 h; 2: With toluene-4-sulfonic acid in toluene 4 h; Heating; Further stages.;
参考文献
Ulgheri, Fausta; Marchetti, Mauro; Piccolo, Oreste
Journal of Organic Chemistry, 2007 , vol. 72, # 16 p. 6056 - 6059
反应条件
sodium hydroxide; hydrogen; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in methanol T=50°C; P=9000.9 Torr; 24 h; Title compound not separated from byproducts.;
参考文献
Ulgheri, Fausta; Marchetti, Mauro; Piccolo, Oreste
Journal of Organic Chemistry, 2007 , vol. 72, # 16 p. 6056 - 6059
反应条件
1: (R)-(S)-Cy2PF-PCy2; copper diacetate; DEMS / tetrahydrofuran; toluene; tert-butyl alcohol / 3 h / 20 °C / |Inert atmosphere 2: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Barancelli, Daniela A.; Salles, Airton G.; Taylor, Jason G.; Correia, Carlos Roque D.
Organic Letters, 2012 , vol. 14, # 23 p. 6036 - 6039