in deuterated toluene
byproducts: Me2PH; standard-vacuum apparatus, 40°C; monitored by NMR;
参考文献
Dehnert, Peter; Grobe, Joseph; Van, Duc Le
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1981 , vol. 36, # 1 p. 48 - 54
→
反应条件
in deuterated toluene
under exclusion of air and moisture in a closed NMR-tube, react. of theCr-complex with (CH3)3SnH in toluene-d8 at 20°C; not isolated, detected by NMR;
参考文献
Grobe, Joseph; Le Van, Duc
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1981 , vol. 36, p. 666 - 671
in further solvent(s)
equilibrium in azoisobutyric acid dinitrile at 40°C; examination with NMR-spectroscopy;;
参考文献
Creemers, H. M. J. C.; Verbeek, F.; Noltes, J. G.
Journal of Organometallic Chemistry, 1967 , vol. 8, p. 469 - 477
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.1.4.6, page 17 - 18
in further solvent(s)
equilibrium in azoisobutyric acid dinitrile at 40°C; examination with NMR-spectroscopy;;
参考文献
Creemers, H. M. J. C.; Verbeek, F.; Noltes, J. G.
Journal of Organometallic Chemistry, 1967 , vol. 8, p. 469 - 477
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.1.4.6, page 17 - 18
