in deuterated toluene
byproducts: (CH3)2AsH; under exclusion of air and moisture in a closed NMR-tube, react. of theMo-complex with (CH3)3SnH in toluene-d8 at 20°C; not isolated, detected by NMR;
参考文献
Grobe, Joseph; Le Van, Duc
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1981 , vol. 36, p. 666 - 671
in not given
byproducts: (CH3)2Sn(CHCF2)2, (CH3)2Sn(CFCHF)2, CF2CHF; reaction in darkness at 70°C;;
参考文献
Beveridge, A. D.; Clark, H. C.; Kwon, J. T.
Canadian Journal of Chemistry, 1966 , vol. 44, p. 179 - 189
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.1.4.4, page 15 - 16
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反应条件
in deuterated toluene
under exclusion of air and moisture in a closed NMR-tube, react. of theCr-complex with (CH3)3SnH in toluene-d8 at 20°C; not isolated, detected by NMR;
参考文献
Grobe, Joseph; Le Van, Duc
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1981 , vol. 36, p. 666 - 671
