in neat (no solvent) Kinetics; (N2); Me3SnH was vac. transferred to stannacyclopentene in NMR tube; sealed; wrapped in Al foil; heated at 89.0°C; NMR monitoring; not isolated;
参考文献
Zhou, Dong; Reiche, Clemens; Nag, Mrinmoy; Soderquist, John A.; Gaspar, Petet P.
Organometallics, 2009 , vol. 28, # 8 p. 2595 - 2608
in benzene-d6 react. of Fe complex and HSnMe3 in benzene, 60°C, 13 h; yields detd. by (1)H-NMR (C5H5Fe(CO)H(SnMe3)2; elem. anal.) and GL-chromy. (other products);
参考文献
Journal of the Chemical Society, Chemical Communications, , # 23 p. 1790 - 1792
