3,4-二苯基-1H-吡咯合成路线 （共 16 条）
反应条件
copper(l) iodide; caesium carbonate; N,N'-dimethylcyclohexane-1,2-diamine in 1,4-dioxane
3 h; Heating;
参考文献
Yuan, Xiyuan; Xu, Xiaobing; Zhou, Xiaobo; Yuan, Jiwei; Mai, Lugen; Li, Yanzhong
Journal of Organic Chemistry, 2007 , vol. 72, # 4 p. 1510 - 1513
反应条件
ethanolamine
1 h; Inert atmosphereReflux;
参考文献
Fukuda, Tsutomu; Koga, Yasuyuki; Iwao, Masatomo
Heterocycles, 2008 , vol. 76, # 2 p. 1237 - 1248
反应条件
1: sodium methylate / methanol / 6 h / 20 °C
2: ammonium chloride / water; N,N-dimethyl-formamide / 20 °C
3: diisobutylaluminium hydride / benzene; toluene / 6 h / 20 °C
View Scheme
参考文献
Ramirez-Rodriguez, Armando; Mendez, Jose M.; Jimenez, Cristina C.; Leon, Fernando; Vazquez, Alfredo
Synthesis, 2012 , vol. 44, # 21 art. no. SS2012M0512OP, p. 3321 - 3326,6
反应条件
1: sodium methylate / methanol / 6 h / 20 °C
2: ammonium chloride / water; N,N-dimethyl-formamide / 20 °C
3: diisobutylaluminium hydride / benzene; toluene / 6 h / 20 °C
View Scheme
参考文献
Ramirez-Rodriguez, Armando; Mendez, Jose M.; Jimenez, Cristina C.; Leon, Fernando; Vazquez, Alfredo
Synthesis, 2012 , vol. 44, # 21 art. no. SS2012M0512OP, p. 3321 - 3326,6
反应条件
1: ammonium chloride / water; N,N-dimethyl-formamide / 20 °C
2: diisobutylaluminium hydride / benzene; toluene / 6 h / 20 °C
View Scheme
参考文献
Ramirez-Rodriguez, Armando; Mendez, Jose M.; Jimenez, Cristina C.; Leon, Fernando; Vazquez, Alfredo
Synthesis, 2012 , vol. 44, # 21 art. no. SS2012M0512OP, p. 3321 - 3326,6
反应条件
1: 71 percent / DBU / tetrahydrofuran / 12 h / Ambient temperature
2: 85 percent / NaOH / ethane-1,2-diol / 2 h / 170 °C
View Scheme
参考文献
Ono, Noboru; Miyagawa, Hirokazu; Ueta, Takahiro; Ogawa, Takuji; Tani, Hiroyuki
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 10 p. 1595 - 1601
