Alpha,Alpha-二甲基苄硫醇合成路线 （共 8 条）
反应条件
sodium methylate in methanol Hydrolysis;
参考文献
Gurudutt, K. N.; Rao, Sanjay; Srinivas, P.; Srinivas, S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1997 , vol. 36, # 12 p. 1169 - 1171
反应条件
Lawesson's reagent in toluene 3 h; Heating;
参考文献
Nishio, Takehiko
Journal of the Chemical Society, Chemical Communications, 1989 , # 4 p. 205 - 206
反应条件
tetrahydrofuran; lithium aluminium tetrahydride
参考文献
Journal of the American Chemical Society, , vol. 77, p. 4255
反应条件
(i) Na2S*5H2O, sulfur, DMSO, (ii) Al-Hg, H2O, THF; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 100, p. 7086 - 7088
反应条件
1: 72 percent / CH2Cl2 / 10 h / Heating 2: 95 percent / sodium methoxide / methanol View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 36, # 12 p. 1169 - 1171
反应条件
1: HCl 2: 72 percent / CH2Cl2 / 10 h / Heating 3: 95 percent / sodium methoxide / methanol View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 36, # 12 p. 1169 - 1171
反应条件
thionyl chloride; thiourea 1.) ether, 2 h, room temp., 2.) ethanol, 2 h, reflux; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 45, # 12 p. 2507 - 2509
反应条件
triethylamine in hexane
参考文献
Mitsubishi Petrochemical Co., Ltd.
Patent: US4343737 A1, 1982 ;
