(价格有效051118)合成路线 （共 35 条）
反应条件
1 Au/TiO2; water in ethyl acetate T=55°C; 3 h;
参考文献
Chemical Communications (Cambridge, United Kingdom), , vol. 48, # 87 p. 10751 - 10753,3
反应条件
Br2 in diethyl ether at room temp.;;
参考文献
Gmelin Handbook: Si: MVol.C, 114, page 320 - 323
反应条件
sodium in neat (no solvent)
T=120°C; 12 h;
参考文献
Gryparis, Charis; Stratakis, Manolis
Chemical Communications (Cambridge, United Kingdom), 2012 , vol. 48, # 87 p. 10751 - 10753,3
反应条件
Na in neat (no solvent)
heating of (C2H5)3SiBr and Na at 140-145°C in a closed vessel;;
参考文献
Kraus, C. A.; Nilson, W. K.
Journal of the American Chemical Society, 1934 , vol. 56, p. 195 - 202
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Gmelin Handbook: Si: MVol.C, 114, page 320 - 323
反应条件
(η5-C5H5)Fe(CO)2Me in N,N-dimethyl-formamide
12 h; UV-irradiation; Product distribution / selectivity;
参考文献
Itazaki, Masumi; Ueda, Kensuke; Nakazawa, Hiroshi
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 3313 - 3316
Angewandte Chemie, 2009 , vol. 121, p. 3363 - 3366
反应条件
(η5-C5H5)Fe(CO)2Me in N,N-dimethyl-formamide
T=25°C; 5 h; Inert atmosphereIrradiation;
参考文献
Itazaki, Masumi; Ueda, Kensuke; Nakazawa, Hiroshi
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 3313 - 3316
Angewandte Chemie, 2009 , vol. 121, p. 3363 - 3366
参考文献
Schumb, W. C.; Saffer, C. M.
Journal of the American Chemical Society, 1939 , vol. 61, p. 363 - 366
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Gmelin Handbook: Si: MVol.C, 114, page 320 - 323
反应条件
1: Br2
2: Na / neat (no solvent)
View Scheme
参考文献
Kraus, C. A.; Nilson, W. K.
Journal of the American Chemical Society, 1934 , vol. 56, p. 195 - 202
反应条件
hydrogen
T=300°C; P=73550.8 Torr;
参考文献
Dolgow; Wolnow
Zhurnal Obshchei Khimii, 1931 , vol. 1, p. 91,101-103
Chem. Zentralbl., 1931 , vol. 102, # II p. 1129
反应条件
hydrogen
T=300°C; P=73550.8 Torr;
参考文献
Dolgow; Wolnow
Zhurnal Obshchei Khimii, 1931 , vol. 1, p. 91,101-103
Chem. Zentralbl., 1931 , vol. 102, # II p. 1129
