(价格有效051118)合成路线 （共 35 条）
反应条件
diethyl ether; Si2Cl6
参考文献
Schumb; Saffer
Journal of the American Chemical Society, 1939 , vol. 61, p. 363,365
反应条件
Hydrogenation.unter Druck bei hohen Temperaturen;
参考文献
Ipatjew; Dolgow
Chemische Berichte, 1929 , vol. 62, p. 1221,1224
反应条件
zinc(II) chloride
T=120°C; 16 h; Yield given;
参考文献
Sidorov, V. I.; Filimonova, M. I.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 4 p. 955 - 956,796
反应条件
phenylacetylene in various solvent(s)
electrolysis;
参考文献
Kunai, Atsutaka; Ohnishi, Osamu; Sakurai, Tomohiro; Ishikawa, Mitsuo
Chemistry Letters, 1995 , # 11 p. 1051 - 1052
反应条件
lithium in tetrahydrofuran
treating of Sb(Si(C2H5)3)3 with Li in THF at room temp. for 107 h, addn. of C6H5CH2Cl, at 50°C for 4 h;
参考文献
Vyazakin, N. S.; Kalinina, G. S.; Kruglaya, O. A.; Razuvaev, G. A.
Zhurnal Obshchei Khimii, 1969 , vol. 39, p. 1964 - 1968
Zhurnal Obshchei Khimii, 1969 , vol. 39, p. 2005 - 2011
Full Text Show Details
Gmelin Handbook: Sb: Org.Comp.2, 1.2.1.1.15, page 55 - 56
反应条件
mercury
72 h; HeatingIrradiation; Yield given. Yields of byproduct given;
参考文献
Brown, Stephen H.; Crabtree, Robert H.
Journal of the American Chemical Society, 1989 , vol. 111, # 8 p. 2946 - 2953
反应条件
in hexadeuterioacetone
Kinetics;
参考文献
Johnson, Curtis E.; Eisenberg, Richard
Journal of the American Chemical Society, 1985 , vol. 107, # 23 p. 6531 - 6540
反应条件
hydrogen
T=300 - 320°C; unter Druck;
参考文献
Ipatjew; Dolgow
Chemische Berichte, 1929 , vol. 62, p. 1221,1224
反应条件
hydrogen in neat (no solvent)
byproducts: propane, n-hexane; High Pressure; heating of (C2H5)3SiCH2CH2CH3 at 300°C under 100 atm H2 for a longer period of time;;
参考文献
Dolgov, B. N.; Vol'nov, Ju. N.
Zhurnal Obshchei Khimii, 1931 , vol. 1, p. 91 - 104
反应条件
hydrogen in neat (no solvent)
byproducts: i-pentane; High Pressure; decompn. at 300°C and 100 atm H2 pressure;;
参考文献
Dolgov, B. N.; Vol'nov, Ju. N.
Zhurnal Obshchei Khimii, 1931 , vol. 1, p. 91 - 104
