(价格有效051118)合成路线 （共 35 条）
反应条件
1: diethyl ether
2: H2 / neat (no solvent)
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参考文献
Gmelin Handbook: Si: MVol.C, 10, page 32 - 34
参考文献
Friedel, C.; Ladenburg, A.
Liebigs Annalen der Chemie, 1880 , vol. 203, p. 241 - 255
Full Text Show Details
Gmelin Handbook: Si: MVol.C, 4, page 14 - 18
参考文献
Woronkow; Chudobin
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 584,586;engl.Ausg.S.629,631
反应条件
disilicon hexaiodide
参考文献
Friedel; Ladenburg
Annales de Chimie (Cachan, France), 1880 , vol. <5>19, p. 401
Justus Liebigs Annalen der Chemie, 1880 , vol. 203, p. 251
反应条件
hydrogen
unter Druck;
参考文献
Ipatjew; Dolgow
Zhurnal Obshchei Khimii, 1931 , vol. 1, p. 6,8,10
Chem. Zentralbl., 1931 , vol. 102, # II p. 1128
反应条件
mercury
2 h; HeatingIrradiationother alkanes; selectivity of cross-dimerization, relative reactivities in cross-dimerizations;
参考文献
Brown, Stephen H.; Crabtree, Robert H.
Journal of the American Chemical Society, 1989 , vol. 111, # 8 p. 2946 - 2953
反应条件
in neat (no solvent)
byproducts: C6H6, SiH4; heating at 350°C for 3 days under H2 pressure;;
参考文献
Ipatiev, V.; Dolgov, B.
Ber., 1929 , vol. 62, p. 1220 - 1226
Full Text Show Details
Gmelin Handbook: Si: MVol.C, 23, page 72 - 75
反应条件
in neat (no solvent)
radiolysis of deoxygenated Et3SiH; various concentrations of EtBr; further unidentified oligomers; GC/MS;
参考文献
Lugovoi, Yu. M.; Getoff, N.
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1989 , vol. 44, # 11 p. 1373 - 1376
反应条件
dihydrogen hexachloroplatinate in isopropyl alcohol
T=100°C; 7 h; various esters, other catalyst, other temp. and time; Product distribution;
参考文献
Voronkov, M. G.; Dubinskaya, E. I.; Dolmaa, G.; Klyba, L. V.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 5 p. 1083 - 1086,958 - 961
参考文献
Lugovoi, Yu. M.; Getoff, N.
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1989 , vol. 44, # 11 p. 1373 - 1376
