2-溴-1-(5-甲基呋喃-2-基)-乙酮合成路线 (共 5 条)
反应条件
bromine in 1,4-dioxane; diethyl ether T=20 - 25°C; Bromination; 0.333333 h;
参考文献
Saldabol; Popelis; Shatz; Slavinskaya
Chemistry of Heterocyclic Compounds, 1999 , vol. 35, # 2 p. 161 - 163
反应条件
ammonium chloride; bromine in 1,4-dioxane; diethyl ether
参考文献
Strohbach, Joseph Walter; Tanis, Steven P.; Moon, Malcolm Wilson; Nieman, James A.; Beauchamp, Thomas J.; Northuis, Jill M.; McGhee, William D.
Patent: US2003/207877 A1, 2003 ;
反应条件
N,N'-diacetylpiperazine hydrogen tribromide in methanol T=40°C;
参考文献
Burakov; Kanibolotskii; Osichenko; Mikhailov; Savelova; Kosmynin
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 9 p. 1210 - 1219
反应条件
N-bromosuccinmide in tetrachloromethane Bromination; 5 h; Heating; Product distribution; Further Variations:SolventsCatalystsTemperaturesReagents;
参考文献
Saldabol; Popelis; Shatz; Slavinskaya
Chemistry of Heterocyclic Compounds, 1999 , vol. 35, # 2 p. 161 - 163
参考文献
PROSKELIA SAS
Patent: WO2006/117211 A2, 2006 ;
Location in patent: Page/Page column 48; 49 ;
WO 2006/117211 A2