2-乙基-2-(羟基甲基)丁醛合成路线 (共 7 条)
反应条件
triethylamine in water 3 h; Heating;
参考文献
Sirkecioglu, Okan; Tahnh, Naciye; Akar, Ahmet
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 2 p. 456 - 460
反应条件
nitrogen oxides containing HNO3; oxygen T=30 - 40°C;
参考文献
Wacker,A.
Patent: DE579308 , 1932 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 20, p. 795
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Wacker,A.
Patent: CH168139 , 1933 ;
参考文献
Wacker,A.
Patent: DE579308 , 1932 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 20, p. 795
反应条件
toluene-4-sulfonic acid T=190°C; 0.0833333 h; Neat (no solvent)Microwave irradiationClosed vessel;
参考文献
Huang, Po-Jung Jimmy; Stanley Cameron; Jha, Amitabh
Tetrahedron Letters, 2009 , vol. 50, # 1 p. 51 - 54
反应条件
1: Py 2: aq. NaOH / methanol 3: H+ View Scheme
参考文献
Janculev,J. et al.
Chemische Berichte, 1967 , vol. 100, p. 715 - 719
反应条件
toluene-4-sulfonic acid T=190°C; 0.0833333 h; Neat (no solvent)Microwave irradiationClosed vessel;
参考文献
Huang, Po-Jung Jimmy; Stanley Cameron; Jha, Amitabh
Tetrahedron Letters, 2009 , vol. 50, # 1 p. 51 - 54
反应条件
1: Py
2: aq. NaOH / methanol
View Scheme
参考文献
Janculev,J. et al.
Chemische Berichte, 1967 , vol. 100, p. 715 - 719