4,4,5,5-四甲基-1,3,2-二氧磷杂环戊烷-2-醇合成路线 （共 23 条）
反应条件
1: 48 percent / H2O / CH2Cl2 / 0.17 h / Ambient temperature 2: 15 percent Spectr. / CDCl3 / 96 h / Ambient temperature View Scheme
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 24, p. 235 - 242
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 41, p. 433 - 438
反应条件
1: 70 percent 2: 26 percent View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 41, p. 433 - 438
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 473,478
Chem.Abstr., , p. 1905
反应条件
in chloroform-d1 96 h; Ambient temperature;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 24, p. 235 - 242
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 41, p. 433 - 438
反应条件
[rhodium(I)chloride(triphenylphosphine)3] in 1,4-dioxane T=100°C; 10 h;
参考文献
Shulyupin, Mstislav O.; Francio, Giancarlo; Beletskaya, Irina P.; Leitner, Walter
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 5 p. 667 - 672
反应条件
potassium tert-butylate in dimethyl sulfoxide T=60°C; 15 h;
参考文献
Bunlaksananusorn, Tanasri; Knochel, Paul
Tetrahedron Letters, 2002 , vol. 43, # 33 p. 5817 - 5819
反应条件
[Pd(allyl)(CH3CN)2][OTf]; C55H37F3O7P2S; NaCH(CO2Me)2 in 1,4-dioxane T=100°C; 18 h; Inert atmosphere; optical yield given as percent eeregioselective reaction;
参考文献
Barta, Katalin; Francio, Giancarlo; Leitner, Walter; Lloyd-Jones, Guy C.; Shepperson, Ian R.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 13 p. 2013 - 2023
反应条件
(2R,4R)-4-Ph2P-2-(Ph2P-CH2)-cyclopentane-C(O)O-tBu; (η3-allyl)(η5-Cp)Pd in 1,4-dioxane T=100°C; Product distribution; Further Variations:ReagentsTemperatures;
参考文献
Shulyupin, Mstislav O.; Francio, Giancarlo; Beletskaya, Irina P.; Leitner, Walter
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 5 p. 667 - 672
